Thermophysical properties of Al2O3.
Abstract
Recently, the performance of solar cell is impacted by rising panel temperatures. For solar cells to work at their best and have the longest possible useful life, the temperature of the panels must be kept at an ideal level. Current temperature sensors have a slow response time, poor accuracy, and low resolution. Meanwhile, Al2O3 and its derivatives have demonstrated a noteworthy role in temperature sensing applications due to its greater surface area, ease of synthesis, tailored optical characteristics, high melting point, and high thermal expansion coefficient. Al2O3-based nanoparticles have been employed in fiber optic-based temperature sensors as a sensing layer, a sensitivity improvement material, and a sensing matrix material. In this chapter, we discuss the function of Al2O3-based nanomaterials in evanescent wave-based temperature sensors, sensing characteristics such as sensitivity, linearity, and repeatability. The ZAZ-based sensor (Section 3.1) shows an operating temperature range between 100.9°C and 1111.0°C, the temperature sensitivity becomes 1.8 × 10−5/°C. The fabricated sensor had a linearity of 99.79%. The synthesized Al2O3 nanoparticles (Section 3.2) were given better linearity and high sensitivity (~27) at 697 nm compared with other sensing materials such as ZnO, SnO2, TiO2. The Al2O3-MgO (50–50%) (Section 3.3) demonstrated an ultrahigh sensitivity of 0.62%/°C with a better linear regression coefficient of 95%. The present advances and problems are also discussed in detail.
Keywords
- Al2O3
- fiber optic sensor
- clad modification technology
- temperature sensor
- solar cell
1. Introduction
Solar energy is one of the more well-known renewable energy sources, and businesses and industries use its energy harvesting techniques extensively. However, one significant disadvantage of commercial solar cells is their low efficiency at higher panel temperatures. The panel temperature, solar radiation, shading, panel inclination, alignment, dust, and maintenance have a significant impact on the energy efficiency of solar cells. A one-degree temperature rise can reduce the efficiency by ~0.045% over a temperature range of 15–60°C in a monocrystalline silicon solar cell [1]. Till now more studies on the use of Al2O3 in solar cells existed. For instance, El-Shafai et al. have prepared a novel hybrid nanomaterial (HNM) (GO@CuO.γ-Al2O3) and studied their thermal and electrical performances. Different nanofluids were prepared from mono NMs (GO, CuO, and γ-Al2O3), and hybrid NMs (GO@CuO, GO@γ-Al2O3, and GO@CuO.γ-Al2O3) with water as a base fluid, to study the thermal conductivity. Different concentrations of the nanofluids (0.0625, 0.125, and 0.2%) were investigated within a temperature range of 20–50°C. Compared to water, GO@CuO.γ-Al2O3 shown maximum enhancement in thermal conductivity (22.56%) with 0.2% concentration and 50°C which is favorable for solar collector heaters. Gunjo et al. have reported that adding 5% of Al2O3 to paraffin-based nanofluids improved the melting rate by 3.46 times and discharge rate by 3 times compared with pure paraffin-based nanofluids. This increases thermal conductivity, dynamic viscosity, and density and also lowers the heat storage compared with pure paraffin-based nanofluids which favors solar energy applications. Khalifa et al. have prepared colloidal Al2O3 nanoparticles by electrolysis method and deposited over p-type silicon wafer by drop casting method and investigated solar cell performances. Mahmoud et al. have studied the performances aluminum oxide (α- Al2O3) nanoparticle and metal aluminate spinel nanoparticle (M- Al2O4, where M is Co, Cu, Ni, Zn) as photo-anodes in quantum dot photovoltaic cells. Electrochemical impedance spectroscopy shows that Zn Al2O4 and Ni Al2O4 nanocomposites have the highest lifetimes of the photogenerated electrons (τn) of 11*10−2 and 96*10−3 ms, respectively, and the lowest diffusion rates (Keff) of 9.09 and 10.42 ms−1, respectively. Amalraj et al. have reported Al2O3 nanoparticles as coolant materials show good efficiency in solar cooling panels. The solar cooling efficiency is 12 and the fill factor is 0.55. However, due to electromagnetic, chemical, and mechanical disturbances, the traditional NTC and PTC-type thermistor, thermocouples, and resistance temperature detectors (RTDs) [2] are unable to give adequate performance for certain real-time applications. Thus, fiber optic sensors would be a superior choice for these applications as the optical signal is immune to electromagnetic field interference, can be used for long-distance communication with low loss, and is compact and simple to employ in real-time applications [3].
Currently, a variety of fiber optic temperature sensors have been reported, including Fabry-Perot, Mach-Zehnder, Fiber Bragg grating, thin film on fiber core, microfiber and coating nanoscale level sensing layer at cladding modified fiber (CMF) and a fiber’s tip [4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15]. Of all, the CMF-based sensors outperform existing ones in all ways, including less weight, electromagnetic interference resistance, ease of manufacture, and increased accuracy in challenging conditions [16]. In CMF, a slight change in the modified nanomaterial due to temperature resulted in light intensity variation. For instance, Huang et al. [15] have reported ZrO2/Al2O3/ZrO2 (ZAZ) coated fiber optic temperature sensor and achieved better sensitivity of 1.8 × 10−5/°C. According to Sun et al. [17], an optical fiber temperature sensor based on temperature cross sensitivity with a RI sensitive device had an improved sensitivity of 350 pm/°C. Rahman et al. [18] have demonstrated bimetallic layer fiber optic temperature sensor and showed moderate temperature sensitivity. Nevertheless, these sensors have their own limitations, such as design complexity, low resolution, poor sensitivity, non-linearity, and dynamic range. By SMO coated CMF, these issues can be resolved.
Till now, a multitude of SMOs has been used in the construction of fiber optic sensors, including ZnO [19], TiO2 [20], SnO2 [21], Al2O3 [22], MgO [23], and SiO2 [24]. A substantial increase in temperature sensor research for improved linearity and sensitivity development has been observed in the last 10 years. Because of their numerous features, nanomaterials have been used in the construction of temperature sensors, greatly advancing the field of temperature sensor research. Due to their exceptional qualities, including a high melting point, a high thermal expansion coefficient, and good physical, chemical, and optical properties, Al2O3 and its nanocomposites have revolutionized the world of sensing. The thermophysical properties (Thermal Conductivity, Viscosity, Density, Specific heat) of Al2O3 nanoparticle were shown in Table 1. In temperature sensors Al2O3-based nanomaterials have been used as a sensing layer, to provide a large surface area and compatibility for temperature detection. In this review, we aim to thoroughly outline the role of Al2O3-based nanomaterials in temperature-based sensors, their present advancements, and challenges.
Material | Density, ρ (Kg/cm3) | Specific heat, Cp (J/Kg K) | Thermal conductivity, k (W/m K) | Viscosity, μ (Kg/ms) |
---|---|---|---|---|
Al2O3 | 981 | 4189 | 0.643 | 0.0006 |
2. Polymer-based fiber optic sensors (PFOS)
Recently, modern technological fields like structural, aeronautical, and aerospace engineering, as automotive, industrial, and medical engineering all heavily rely on sensors. However, till now most of the sensors are based on electrical transduction mechanism. Besides that, sensors based on optics facilitate multitude of benefits such as flexibility, anti-electromagnetic interference, low cost, and easy fabrication compared with conventional electrical sensors. The use of polymer-based fibers in the manufacture of sensors allows the researcher to create any type of fiber geometries, which is a problem with glass fiber that has not yet been resolved. Another advantage of polymer-based fiber optic sensors is the ease with which they can be modified by imprinted polymers. Materials are also another important key parameter for polymer-based optical fiber fabrication and it can be divided into two categories: plastic and natural materials. Poly(methyl methacrylate) (PMMA), cyclo-olefin polymer (COP, ZeonexTM), polycarbonate (PC), amorphous fluoropolymer (CYTOPTM), and PDMS (polydimethylsiloxane) are the most common materials for polymer-based optical fiber fabrications (Chemosensor). The fiber can be made from a single material or a combination of polymer materials when cladding and core are made from different materials. Generally, these polymers-based optical fibers provide good optical and mechanical properties, ease of access, and use [25]. POF can be produced as a single-mode [26, 27] and multimode fiber [28, 29], with a step [30] or gradient index refractive index profile [31]. The fiber has opened up a broad number of uses depending on the type of fiber, diameter of the core/cladding, refractive index of the core/cladding, numerical aperture, and dopants utilized in the fabrication process. Figure 1 shows the record of research articles in the database Scopus.
2.1 POF temperature sensing
Basically, the fiber optic sensor consists of the light source, sensor element, and detector which can be further interfaced with the data acquisition device (Figure 2). An optical fiber (single-mode or multimode) is used to direct a light source, such as a laser (narrowband source), LED (broadband source) to the spectrometer, where optical signal variations will be the measurable quantity of interest (Temperature). The temporal or spectral domains can be used to analyze the measurement signal. A photodiode and an optical spectrum analyzer or a spectrometer can be used as the detection system [33]. Generally, POF sensors offer distributed [34] and pointwise sensing measurements. However, owing to high attenuation, the POF sensors are dedicated mainly to pointwise measurement. Temperature sensing by the POF sensor can be an interaction of temperature parameter that causes changes in the intensity (amplitude), frequency, phase, and polarization of the transmitted light [35, 36, 37].
2.2 Evanescent wave absorption in optical fiber
Typically, synthesized nanoparticles (ηAl2O3 = 1.763) were used in the CMF sensor to replace the natural cladding (ηclad = 1.402). As a result, the sensor enters a leaky mode known as ηmclad> > ηcore, which results in a reduction in propagated light intensity. The evanescent absorption in the modified cladding’s changing refractive index could be the cause of the output light’s temperature-dependent intensity variation. When the light was guided through the fiber under total internal reflection at the core/modified cladding interface, a portion of the light was transmitted into the modified cladding region, where a portion will be reentered back for propagation based on the change in the modified cladding’s refractive index and the rest will be lost. The intensity of this phenomenon, known as an evanescent field, decreases exponentially the farther it is from the surface [38]. When atmosphere temperature varies, the light intensity that travels through the fiber changes as a result of changes in modified cladding refractive index which affects sensor output. The crux of temperature sensing is mainly due to changes in refractive index because of the thermal expansion and thermo-optic effect [39, 40].
2.3 Al2O3 nanomaterials for temperature sensing
The development of nanotechnology over the past 10 years has greatly sparked interest in every area of science and technology. In order to create novel materials, nanotechnology has been primarily used to reorganize bulk materials at the nanoscale. Al2O3-based nanoparticles, among other forms of nanomaterials, have drawn a lot of interest from the scientific community because of their exceptional qualities, including a high melting point, a high thermal expansion coefficient, and good physical, chemical, and optical properties. Both amorphous and crystalline phases can be found in aluminum oxide, often known as alumina (Al2O3). The crystalline form of Al2O3 has a number of metastable structural phases, including corundum, which is a stable phase with a rhombohedral structure, as well as the following: Al2O3 (monoclinic structure), Al2O3 (orthorhombic structure), Al2O3 (cubic or hexagonal structure), Al2O3 (tetragonal structure), and Al2O3 (orthoclinic structure). Aluminum (Al3+) ions and vacancies are randomly distributed throughout tetrahedral (AlO4), polyhedral (AlO5), and octahedral (AlO6) sites in amorphous Al2O3 [41, 42]. Numerous papers describe the use of Al2O3 and its composites in applications for gas sensing, environmental analysis, and temperature sensing.
2.4 Synthesis of Al2O3 nanomaterials
The synthesis of Al2O3 is done by various approaches such as sol-gel, PVD, CVD, hydrothermal, co-precipitation, solvothermal or sonochemical methods [43, 44]. Co-precipitation is one of these methods, and because of its capacity to produce large quantities of Al2O3 nanostructure at a low cost and with no environmental impact, it has the potential for application in this process. Co-precipitation was employed to synthesize Al2O3 nanoparticles. In a nutshell, 50 ml of distilled water was mixed with 2.12 g (0.2 M) of Al (NO3)2. 9H2O precursor, and the mixture was vigorously agitated for 2 hours. Drop by drop, 10 ml of 2 M NaOH stock solution was added to the previously combined solution while being constantly stirred until the pH level reached 8.0. The reacted solution was additionally left at room temperature for 24 hours. The white precipitate that resulted was then washed three times. The resultant nanoparticles were filtered and calcinated at 600°C for 4 h.
2.5 Sensor region preparation
Figure 3 depicts the schematic diagram of the metal oxide-coated temperature sensing system. The transmitted light spectra of our proposed sensor were studied using a broadband light source (SLS201/M) and an optical spectrometer. The cladding modification method was used to achieve a fiber optic temperature sensor probe (CMM). A central portion of a PMMA optical fiber was denuded and etched with an acetone solution. The synthesized metal oxide nanoparticles were mixed with double distilled water to form a paste, which was then deposited in a dip coating technique to the etched surface to a thickness of 20 μm (Figure 4). The coated optical fiber was then allowed to dry at ambient temperature and employed as a sensing region. The sensor was kept in a temperature-sensing chamber, and a heater coupled with microcontroller was used to regulate the temperature. The holder was used to clip the two ends of the fiber, preventing interference from outside disturbances. Glue was used to firmly seal the sensor chamber [46].
3. Assessment of temperature sensing performances
3.1 Al2O3 nanomaterials-based temperature sensor
In this chapter, the sensor head was built with three layers of ZrO2/Al2O3/ZrO2 (ZAZ) dielectric materials via physical vapor deposition (PVD) onto the tip of a sapphire fiber [15]. The sensor was held within a high-temperature furnace for temperature sensing following ZAZ deposition and thermal annealing. As seen in Figure 5, a 3 dB multimode optical fiber coupler, a k-type thermocouple, a broadband light source, and a fiber optic spectrometer were all used in the measurement. Due to the thermo-optic and elastic-optic effects, the refractive index and thickness of the ZAZ films will rise as the ambient temperature rises.
This will cause the interference spectra to shift and the optical path difference (OPD) of the thin film interferometer to vary. Additionally, a rise in the ambient temperature will cause the interference spectra to shift. As a result, it is possible to measure the ambient temperature. When the ambient temperature changes from 100.9 to 1111.0°C, the temperature sensitivity becomes 1.8 × 10−5/°C. The fabricated sensor had a linearity of 99.79%.
3.2 Fabrication of fiber optic-based temperature sensor with various metal oxides (ZnO, SnO2, Al2O3, and TiO2) as sensing layer
The co-precipitation approach was used in this study to synthesize metal oxide semiconductors (ZnO, SnO2, Al2O3, and TiO2), which were then subjected to several material characterization techniques [47]. According to the XRD data, the ZnO nanoparticle crystallized in a hexagonal wurtzite structure, while SnO2 nanoparticles are in a rutile tetragonal structure, Al2O3 nanoparticles are in a rhombohedral structure, and TiO2 nanoparticles are in a rutile anatase structure. The SEM analysis confirms that all of the synthesized nanopowders are in grains that are dispersed equally (Figure 6). Additionally, dip coating was used to deposit the synthesized metal oxide semiconductors over the optical fiber’s cladding-modified region, and investigated temperature sensing for broad wavelength range and specific wavelength ranges (Blue, Green, Orange, Red, and Yellow). Figure 7 depicts the change in light intensity of metal oxide nanoparticles (ZnO, SnO2, Al2O3, and TiO2) at various temperatures between 35 and 75°C with a 5°C step interval.
The three characteristic peaks appear in the spectrum at wavelengths of 697, 774, and 952 nm respectively which are the characteristic spectrum of the optical fiber used. The characteristic spectrum shows intensity variations at various temperatures. In comparison to the other two characteristic peaks, the temperature variation led to the greatest peak intensity variation at about 697 nm. Figure 8 depicts the variation in light intensity of Al2O3 nanoparticles at various temperatures, from 35 to 75°C with a step interval of 5°C (Blue, Green, Orange, Red, and Yellow). When compared to other wavelengths, it has been shown that blue and orange wavelengths displayed a significant variation in intensity. It shows that both blue and orange wavelength ranges are possible for the manufactured fiber optic temperature sensor to operate in. It reveals that the synthesized Al2O3 nanoparticles were given better linearity and high sensitivity (~27) at 697 nm compared with other sensing materials. Further, wavelength dependent temperature sensing characteristics of Al2O3 nanopowders were studied and it shows better sensitivity (~34) in the blue wavelength region (450 nm–495 nm) (Figure 9).
3.3 Fabrication of fiber optic-based temperature sensor with Al2O3, MgO, and composites as sensing layer
Fabrication and characterization of fiber optic temperature sensors using Al2O3-MgO nanocomposite as cladding material have been reported [45]. To synthesize Al2O3, MgO, and their various compositions, the co-precipitation technique was chosen and subjected to various material characterizations. From, XRD, Al2O3 and MgO nanoparticles are in rhombohedral structure and cubic structure and Al2O3-MgO nanocomposite conceives both rhombohedral and cubic crystal structure. The SEM morphology of Al2O3, MgO, and Al2O3-MgO (25–75%, 50–50%, 75–25%) composite nanopowders showed non-uniform agglomerated nanoparticles. The EDS analysis addresses the distribution of Al, Mg, and O elements, respectively in Al2O3-MgO nanocomposite. The unclad part of an optical fiber was coated with Al2O3, MgO, and Al2O3-MgO nanocomposites to create the temperature sensor probe. The temperature sensor response has been studied in the temperature range of 35–80°C (Figure 10) and Al2O3-MgO (50–50%) composite demonstrated an ultrahigh sensitivity of 0.62%/°C with a better linear regression coefficient of 95% (Figure 11). Further, the fabricated sensor emphasizes the feature of compact sensing structure, high-temperature sensitivity, good linearity, and wide temperature measurement range.
4. Challenges and future prospects
The future development of fiber optic temperature sensor faces challenges and opportunities, such as: (1) The development of new high-temperature-resistant optical fiber with excellent material and mechanical properties improving the temperature range of the sensor; (2) Adding durable cladding to crystal fiber highly enhances the sensing performance and long-term stability and (3) The development of sensors with multi-parameters sensing is essential along with better stability and package protection.
5. Conclusion
In summary, Al2O3-based nanomaterials have attracted significant attention of the scientific community for the fabrication of fiber optic-based temperature sensors due to their distinct electrical, mechanical, thermal, and optical properties. This article has discussed the crucial function of Al2O3-based nanomaterials in evanescent wave-based temperature sensors, as well as their present advancements and difficulties. Al2O3-based nanoparticles serve as a better sensing layer, sensitivity enhancement material, and sensing matrix material in fiber optic-based temperature sensors.
Acknowledgments
The authors would like to express their heartfelt gratitude to the Department of Science and Technology (DST), New Delhi, India, for providing financial assistance through the FIST (Fund for Improvement of S&T Infrastructure in Higher Education Institutions) project [SR/FST/ETI-015/2011].
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