Chemical compositions of P91 steel (wt%).
Abstract
Previously, we have proposed creep deformation law estimated by non-dimensional time representation to predict creep fracture and remnant life. Furthermore, using steady state creep rate coupled with crack growth rate law based on Q* parameter, QL* parameter was derived and it was found to enable us to discriminate creep ductility and predict creep fracture life. In this study, a quantitative estimation and a prediction methods of mechanical performance on creep strength (MPCS) and creep fracture life of the creep ductile materials including a weld joint notched specimen was noticed and the following studies were conducted. 1) The similarity law of creep deformation, 2) QL*map, which discriminates creep ductility and predicts creep fracture life, 3) Derivation method of mechanical indicators, “Converted stress”, and ∆QL*, which quantify MPCS, 4) Example of the quantitative estimation by these parameters using P91 steel and its weld joint notched specimens. From these results, the concept of the converted stress and the ∆QL*were found to enable us to conduct quantitative estimation of MPCS and prediction of creep fracture life, with the short experimental period, the small number of specimens, the reasonable accuracy and an economic efficiency, which is an engineering significance.
Keywords
- QL*
- MPCS
- converted stress
- creep ductility
- weld joint
- creep fracture life
- ∆QL*
1. Introduction
Concerning the estimation of mechanical performance on creep and creep-fatigue interaction, the law on the relationship between applied stress and fracture life [1], the Larson-Miller parameter [2], the Manson-Coffin law [3, 4] and the Ω method [5] were proposed for a smooth specimen. Furthermore, from the point of the application to actual engineering structure, the prediction of the crack growth life originated from a site of stress concentration is important and the establishment of the law of creep crack growth rate to predict creep crack growth life has been conducted [6, 7]. Especially, the establishment of the quantitative estimation method on the mechanical performance for a weld joint specimen under creep condition is important, because the effect of the morphology of heat affected zone (HAZ) line and the difference of material structure, between the weld metal, HAZ and the base metal, on the creep fracture life are significant factors to predict the creep fracture life [8].
Furthermore, from the point of actual application under recent social demand, such as the short experimental period and economical situation, it is necessary to establish the predicting method of creep fracture life by using small number of specimens and by conducting the short life creep test.
In this study, under these social demands mentioned above, by using a notched specimen of creep ductile material, the methods of estimating the quantitative mechanical performance on creep strength (MPCS) and of predicting creep fracture life of the weld joint by using small number of specimens and by conducting the short life creep test were proposed.
2. Theoretical foundation and background
2.1 Similarity law of creep deformation
For creep ductile materials, the time sequential characteristic of creep deformation plotted against non-dimensional time controlled by each fracture life,
where
2.2 Evaluation method of creep ductility (QL * parameter)
The creep crack growth rate (CCGR) is written by
By integrating Eq. (2) and (3), the life of creep crack growth is written by Eqns. (4) and (5),
where
The steady state creep strain rate is given by the Eq. (6).
Dividing Eq. (6) by Eq. (5),
Where
For creep ductile materials, since steady state creep rate well correlates with the inverse value of fracture life, values of
Based on the
2.3 Derivation method of the converted stress and ∆ QL ∗
For the case of creep ductile materials such as Cr-Mo-V steel, the similarity law of creep deformation and Eq. (8) described in the Section 2.1 and 2.2 are valid [11, 12]. For such case, the concept of the converted stress is defined and valid to conduct a quantitative estimation of the MPCS and the prediction of creep fracture life.
This section shows the derivation method of the converted stress. When the same similarity law of creep deformation is valid both for A and B materials, the relationship between
The flow chart of the derivation method of the converted stress is shown in Figure 5.
When the similarity law of creep deformation is valid, Eq. (8) is unique both for A and B materials and it was written by Eq. (9),
where
Steady state creep rate for the A material is experimentally given by Eq. (10).
Using Eqns. (9) and (10),
where
When the steady state creep rate,
Substituting
where
The converted stress of the B material into that of the A material,
Furthermore, the converted stress ratio,
where
For the case of
For the case of
In addition, the concept of
Schematic illustration of experimental characteristics of
Using the concept of the converted stress and
3. The prediction of creep fracture life and the derivation of the converted stress to estimate the mechanical performance of creep strength of a double edge notched weld joint specimen for P91 steel based on the QL * concept
3.1 Material and specimen
The material used for this study is P91 steel and matching weld metal of US-9Nb, which is a similar material as P91 steel. The chemical composition and mechanical properties are shown in Tables 1 and 2.
C | Si | Mn | P | S | Ni |
---|---|---|---|---|---|
0.08–0.12 | 0.2–0.5 | 0.3–0.6 | <0.02 | <0.01 | <0.40 |
Cr | Mo | V | Nb | Al | N |
8.0–9.5 | 0.85–1.05 | 0.18–0.25 | 0.06–0.10 | <0.04 | 0.03–0.07 |
Tensile stress (MPa) | 0.2% proof stress (MPa) |
---|---|
590 | 410 |
The specimen used is a double-edge notched specimen (DEN) as shown in Figure 2. Sampling sites of specimen of base metal and weld joint are shown in Figure 7.
3.2 Experimental method
The machine system was designed and developed to enable automatic real-time observational experiments using a CCD microscope [15]. Now, CCD microscope was replaced to digital microscope manufactured by KEYENCE corporation. Using this apparatus, in situ observation of creep damage progression was conducted and the images of the damage region were quantified using a PC. The tests were conducted under high temperature vacuum conditions of 10−4 Pa. The creep damage region around the notch tip was found to be a dark region, composed of voids and micro-cracks originating along grain boundaries, as shown in previous results for SUS304 stainless steel [10, 15]. The dark region is defined as a creep damage region owing to the following reasons.
The specimens were heated using infrared rays (IR) under vacuum conditions, as shown in Figure 8. Creep damage is caused by micro-cracking along a grain boundary, which is composed of voids at the grain boundary [10, 15] that are considered to be caused by vacancy diffusion [16, 17]. In the damage region, a specimen surface becomes irregular due to micro-cracking along a grain boundary. In this region, diffused reflection of light by the lamp of IR was caused and it shows as the dark region.
3.3 Experimental conditions and results
Previously, experimental results were published in Japanese [18], however, more detailed analyses are needed by more accurate analyses. In this section, updated results are written.
3.3.1 Similarity law of creep deformation
Experimental conditions, their results of steady state RNOD rate and creep fracture life are shown in Table 3. These results show that the fracture life of weld joint takes 3.5 ∼ 5% of that for the base metal.
No. | Temp. (°C) | Stress (MPa) | Steady state RNOD rate (1/hr) | Creep fracture Life | |
---|---|---|---|---|---|
Weld joint | W-1 | 650 | 135 | 5.65 × 10−2 | 9.5 |
W-2 | 113 | 9.00 × 10−3 | 55.1 | ||
W-3 | 113 | 2.00 × 10−2 | 23.0 (predicted) | ||
Base metal | B-1 | 650 | 200 | 1.13 × 10−1 | 4.0 (predicted) |
B-2 | 135 | 1.62 × 10−3 | 183.6 | ||
B-3 | 113 | 1.44 × 10−4 | *1550.0 |
Non-dimensional time sequential characteristics of the RNOD curve (creep deformation) controlled by each fracture life are shown in Figure 9. For the base metal, the similarity law of RNOD curve caused, which is independent of applied stress. For the weld joint, the similarity law also caused for the case of
3.3.2 Damage progression behavior of the notched specimen of the weld joint and the base metal
The time sequential behavior of damage progression around a notch tip of the weld joint specimen for P91 steel observed by the in situ observational testing machine under creep condition with a temperature of 650
The time sequential behavior of damage progression around a notch tip of the base metal observed by the in situ observational testing machine under creep condition with a temperature of 650
For the base metal, creep damage originated from a notch tip in the direction of shearing stress. When the damage area spread over the specimen width, final fracture occurred. However, damage progression behavior is different from that of the weld joint, creep fracture mechanism is also creep damage dominant, which also related to the similarity law of creep deformation as is mentioned in the Section 3.3.1.
3.3.3 Experimental law of creep fracture life and creep strain rate
As shown in Figure 12, a unique linear logarithmic relationship between creep fracture life and steady state creep strain rate, that is, the unique
As shown in Figure 13, the linear logarithmic relationship between the steady state creep strain rate and the applied stress was found out both for the base metal and the weld joint respectively.
From these experimental results, the following equations are obtained.
where
3.3.4 The derivation of the converted stress and the converted stress ratio
As shown in Figure 12, the
As shown in Figure 13, the linear logarithmic relationship between the steady state creep strain rate and the applied stress is given by Eq. (16) for the base metal.
Substituting Eq. (16) into Eq. (15), Eq. (18) is obtained for the base metal.
where
Using the experimental results of steady state creep strain rate,
Substituting
The converted stress ratio,
The accuracy of predictive creep fracture life of the weld joint derived from the
Applied stress(MPa) | Creep fracture life (hr) of the base metal, | Converted stress(MPa), | Converted stress ratio,η | Ratio of fracture life of weld joint to that of base metal, | |
---|---|---|---|---|---|
Base metal | 135 | 183.6 | 135 | 1.0 | 1.0 |
Weld joint | 9.5 | 187 | 1.39 | 0.052 | |
7.2 (predicted by | |||||
Base metal | 113 | 1519.3 | 113 | 1.0 | 1.0 |
Weld joint | 55.13 | 160 | 1.41 | 0.035 | |
39.3 (predicted by |
The value of the converted stress ratio of the weld joint into that of the base metal,
From these results, the converted stress ratio is more accurate indicator of estimating the MPCS than the fracture life ratio from the point of the data scattering.
For creep ductile materials, the prediction of the creep fracture life of the target materials and the quantitative comparative estimation of the MPCS of the target materials to the control material are found to be possible measuring the steady state creep rate of the target materials by the short time range experiments.
4. Discussions
4.1 Application of this theory to the case of C (T) specimens of the weld joint for P91 and P92 steels
The
These results showed that the
4.2 Application of this theory to the case of a smooth specimen and a notched specimen
The
These results showed that the
5. Summary
The experimental law on the relationship between the steady state creep rate and creep fracture life given by Eq. (21) was well known as the Monkman – Grant law [19], however, Yokobori, et al. showed this law is only valid under limited case, and the data band is essentially different depending on the creep ductility as shown in Figure 3 [11].
Furthermore, however the similar equation as Eq. (21) was found to be valid for creep ductile materials and it was correctly written by Eq. (8).
In this study, for creep ductile materials,
On the basis of these results mentioned above, the prediction of the creep fracture life and the quantitative estimation of the MPCS were found to be possible using the
The experimental data obtained by the commissioned research with Tohoku Electric Power Co.Inc. from April 2016 to March 2019 were used in the section of 3.3 in this proof [20].
Acknowledgments
Parts of this work was supported by Council for Science, Technology and Innovation (CSTI), Cross-ministerial Strategic Innovation Promotion Program (SIP), “Materials Integration for revolutionary design system of structural materials” (Funding agency: JST).
Conflict of interest
The author declares that there is no conflict of interest associated with this study.
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