Open access peer-reviewed chapter

# Variational Calibration

By Michael Surdu

Submitted: September 30th 2017Reviewed: January 19th 2018Published: August 1st 2018

DOI: 10.5772/intechopen.74220

Downloaded: 316

## Abstract

The approach to the improving the accuracy of the impedance parameter measurements is described. This approach is based on the well-known variations of the influence of the disturbing factors on the results of measurement. Using these variations, measurement circuit provides the additional number of measurements, equal to the number of the disturbing factors. System of equations describes these results of measurements. The solution of this system eliminates the influence of the appropriate uncertainty sources on the results of measurement and gets the true result of the measured value. In addition, the solution of this system also gets the values of the uncertainty components in every measurement and possibility to monitor the properties of the measurement circuit. Examples of the realization of this method for improving the accuracy of the impedance parameter measurements in different bridges are given.

### Keywords

• impedance
• variation calibration
• uncertainty
• measurement
• algorithm
• comparison
• quadrature
• standard
• digital synthesis
• frequency range
• transfer’s function

## 1. Introduction

History of the electricity science is the history of the development, in sufficient part, of the new methods of measurements. These methods are described perfectly well, for example, in [1]. Widely used replacing and substitution methods entered in all handbooks [2]. Bridge methods are described in many monographs [3, 4]. Monographs [5, 6] describe different methods of bridges’ accurate balance. Many methods of uncertainty correction are described in [7, 8]. All these methods have their widely discussed advantages and disadvantages. There exists no method that could decide all problems, which appears in measuring practice. This chapter describes the method of the variational calibration [9] in the impedance measurements. This method is based on the sequential variation of the influence of the disturbing factors on the results of measurement. System of equations describes these results. Solution of this system eliminates influences of the disturbing factors and gets the accurate results of measurement. This method significantly simplifies the accurate devices, reducing their weight, dimension and cost, but increases the time of measurement.

## 2. The variational calibration

### 2.1. Theoretical basis of the variational calibration

Every measuring circuit (MC) has the input value, which has to be measured and generates measured output value. In an ideal case, the results of measurement depend on the input value and the transfer function k of the MC only.

Formula (1) describes the result of measurement of ideal MC:

Zx=kZ0E1

Formula (2) describes the standard uncertainty δidof such measurement:

δid=δ02+δs2E2

Here δ0 and δs are the uncertainties, of the standard Z0 and the uncertainty, caused by the sensitivity of the MC.

In the real MC, the results of measurement Ζx0 also depend on the complex of the disturbing factors z1zizjas well (for simplicity of the description, these factors on the Figure 1 are shown being out of MC). These factors create proper complex of the uncertainties of measurements δ1…δi …δj and shift the appropriate result Zx0of measurement from its ideal value Zx. The much more complicated mathematic model (3) of the real MC now describes the results of measurement:

Zx0=γZxδ1δiδjδ0δsE3

Usually the model (3) is well known from preliminary investigations of the MC.

In the simplest case, every disturbing factor z1..zi..zjcreates appropriate uncertainty components δ1δiδj. In more complicated cases, some disturbing factors z1zican influence some complex ZiZi+mof the results of measurement. But we know functions δi=fiz1ziznand do not know just the constant coefficients, which enters into these dependences.

Formula (4) describes the standard uncertainty δr of the measurement of the real MC:

δr=δ02+Σ1jδi2+δs2E4

To eliminate the influence of the uncertainties δ1…δi…δj on the results of measurement, the variation method was developed (VM) [9]. Figure 2 illustrates this method. Here, MC contains n additional variators V1…Vj. Last ones influence the uncertainty sources z1…zj and change the uncertainty δ1…δj. It creates the output of the proper results of MC measurement Zx1…Zxj.

Variators cannot change the uncertainties δ0 and δs. These uncertainties are supposed to be known or equal to zero during the VM calibration.

VM consists of the following steps:

1. First, MC measures initial value Zx0 of the input value Zx.

2. Then, MC consequently varies the influence of the disturbing factor zi on the well-known value αi.

Variations could be provided in any order. To simplify the system of equations, it is preferable to perform variations sequentially and to switch ON the variation αi when all other variations are switched OFF.

Variations could have any law. To simplify the system of equation, it is preferable to provide the multiplicative variation (when we multiply the appropriate uncertainty component δi on well-known ratio αiiv = αiδi)) or additive variation (when we add the appropriate well-known uncertainty Δv to the uncertainty component Δimiv = Δim + Δv)).

3. After every variation, MC measures the results of the measurement Zx1…Zxi…Zxj.

4. The system of Eqs. (5) describes these measurements:

Zx0=γZxδ1δiδjδ0δsZx1=γZxδ1α1δiδjδ0δsZxj=γZxδ1δiδjajδ0δsE5

The system (5) contains j + 1 unknown quantities: Zx and uncertainties of measurement δ1…δj, and j + 1 results of measurement Zx0…Zxj. Solution (6) of this system gets the true value of the results of measurement Zx and the values of the uncertainties δ1…δj of the measurement:

Zx=ρ0Ζx0Zxjα1αjδ0δsδ1=ρ1Ζx0Zxjα1αjδ0δsδj=ρjΖx0Zxjα1αjδ0δsE6

Periodical variation calibration lets us to observe the behavior of every disturbing factor, to determine their stability, to monitor measuring circuit and to ensure precision of the period of the variational calibration.

Let the uncertainty caused by the finite sensitivity of the i-measurement be δsi and the uncertainty of the variation αi be δαi. In this case, formula (7) describes the resulting standard uncertainty δc of the measurement with variation calibration:

δc=δ02+Σ0jδi2δαi2+δsi2E7

Eq. (7) shows that the VM sharply decreases influence of the uncertainty components δi on the common uncertainty of measurement (on the 1/δαi times).

Let us suppose uncertainty source zi creates uncertainty δi = 10−3 and we need to decrease it to the value 10−6. It means that we have to provide appropriate variation with uncertainty better than 10−3 only. It is a very important result of the VM. This effect is restricted only by the stability of the uncertainties δ1…δj during the time of measurement.

Let us suppose that time of every measurement is ti. It means that the common time tc of measurement increases to the value:

tc=Σ0jtiE8

Let us suppose that δαi = 0 and δ0 = 0. In this case, formula (9) describes the standard uncertainty of measurement caused by sensitivity of measurements only:

δc=Σ0jδsi2.E9

Formulas (8) and (9) show that the variation method has two disadvantages:

• Variation method needs n + 1 measurement instead one only. It sufficiently increases the time of measurement.

• Variation method increases the contribution of measurement sensitivity δsi in the common uncertainty of measurement.

We can overcome these two disadvantages of the variation method in different ways. Here, we shortly describe time and space clustering of the thesaurus of the uncertainty sources.

#### 2.1.1. Time clustering

Usually, different uncertainty sources have different typical speeds of drift. We can divide the thesaurus of j uncertainty sources into clusters, which have congruous time of drift. Figure 3 illustrates this approach. In Figure 3, thesaurus of the j uncertainty components is divided into three clusters T1, T2 and T3 (j = m + n + k).

The first cluster (T1) joins m of the most stable uncertainty sources. It could be instability of the internal standards or arms ratios in transformer bridges, and so on. MC provides their calibration very seldom, for example, one time per year. For this calibration, MC performs sequential variation of all sources of uncertainty and provides m + n + k + 1 measurements. The system (5) of equations describes the results of these measurements. Solution (6) of this system gets us values of the m uncertainties of the first cluster.

The second cluster (T2) joins the n less stable sources of the uncertainty. It could be the temperature dependences of the operational amplifiers parameters, and so on. Calibration of these sources is provided more frequently, for example, one time per hour. During this calibration, we suppose that the m uncertainties of the first clusters are stable. Values of these uncertainties enter in the system (5) as constants. To find values of the n uncertainties of the second cluster, MC varies sequentially the uncertainty sources n + k, provides proper measurements and solves the system (5). It needs n + k + 1 measurements.

The third cluster (T3) joins the k uncertainty sources which change most quickly. This cluster mostly includes the sources, which directly depends on the parameters of the object to be measured. This calibration is aimed to find the true results of measurement and values of the last k uncertainties. During this calibration, we suppose that uncertainties of the first and second clusters are stable. Their appropriate values are entered in system (5) as constants. Calibration now consists of sequential variation of the k uncertainties of third cluster and appropriate measurements. Solution of the system (5) gets us the true results of measurement Zx and last k uncertainties. This calibration needs k + 1 measurements only.

Let us suppose that any measurement needs time ti. Formula (10) describes the weighted average tc of the measurement with variation calibration:

tc=Σ1kti1+n+km+n+kTkTm+km+n+kTkTmE10

where Σ1ktiis the time of the k cluster calibration and measurement, Tn/Tmis the ratio of the periods of the second Tn and first Tm clusters calibrations and Tk/Tmis the ratio of the periods of the third Tk and first Tm cluster calibrations.

Formula (10) shows that the time of measurement decreases only slightly during the time of calibration of the third cluster. It means sufficient diminution of the time of measurement.

#### 2.1.2. Space clustering

Sometimes, we do not need to separately study every component of the measurement uncertainty. In this case, we use space clustering. During the space clustering, MC is represented as a complex of the n quadripoles and standards to be compared. Figure 4 shows such decomposition of the measurement circuit.

In Figure 4, K1 … Kn are the quadripoles of the MC and the V1…Vn are the variators used to vary the transfer coefficient of the proper quadripole.

The following formula describes the decomposed MC:

Zx0=fZxK1ΔK1KiΔKiKnΔKnE11

where Zx and Zx0 are the MC input and output values, respectively, ΔΚ1… ΔΚi… ΔΚn are the uncertainties of the quadripole transfer coefficients K1KiKn.

The following formula expresses the dependence of the measurement uncertainty δr on the components of the decomposed MC:

δr=δ02+δs2+Σ1nΔKi2E12

where δs is the uncertainty caused by the finite MC sensitivity.

Let us provide n well-known variations ν1νiνnof the quadripole transfer coefficients K1KiKn. MC provides the new measurements Zx0…Zxi…Zxn of the unknown value Zx after every variation. The system of Eq. (13) describes these measurements:

Zx0=fZxK1ΔK1KiΔKiKnΔKnZx1=fZxK1ΔK1v1KiΔKiKnΔKnZxn=fZxK1ΔK1KiΔKiKnΔKnvnE13

Solution of the system (13) of equations gets accurate results of measurement together with all uncertainties of the quadripoles.

Formulas (8) and (9) describe the uncertainty and time of measurement when using the space clustering as well. However, the number of measurements in case of space clustering is much less. Error accumulation and common time of measurement are much less as well.

We can decompose the measuring circuit in different ways. Optimal decomposition depends on the structure of the measuring circuit. Here, it is impossible to analyze all these possibilities. In most cases, we are forced to use time and space clustering together.

It should be noted that variation method was used earlier in some measurements (e.g., elimination of the uncertainty caused by self-heating of the resistive thermometer in temperature measurements). Here, we consider generalization and dissemination of this method in different areas, first in impedance measurements.

### 2.2. Experimental developments of the VM

VM was used in several developments. It is too complicated to analyze all these possible applications. Here, we consider only some applications of this method in very important cases of widely used digibridges and in accurate transformer bridges.

#### 2.2.1. Application of the VM in digibridges

Development of the integral operational amplifiers and microprocessors resulted in the new class of measuring devices—digibridges [10, 11, 12]. Nowadays, digibridges cover most part of the specific market of the impedance meters. Now many companies manufacture digibridges (HP, Agilent, TeGam, IetLab, Wine Kerr, etc).

#### 2.2.1.1. Operation and analysis

A usual digibridge consists of two serially coupled impedances Zxand Z0(see Figure 5) These impedances are connected between outputs of the generator G and the protecting amplifier A. Negative input of this amplifier is connected to the common point of the impedances Zxand Z0. Amplifier A creates in this point the potential, close to zero (virtual ground). The same current Ixflows through both impedances Zxand Z0 and creates voltages Uxand U0. Differential vector voltmeter DVV, through switcher S0, measures these voltages and transfers the results of measurement to microcontroller μC. μC controls the operation of the ΜC, processes results of the voltages measurements and calculates the ratio of two impedances Zxand Z0. Display D shows results of measurements.

The amplifier A protects measuring circuit and decreases the influence of the parasitic admittance Ycbetween the amplifier inputs on the results of measurement.

In case if gain K is infinite, Eq. (14) describes the process of measurement:

Zx/Z0=Ux/U0E14

Let gain K be finite. In this case, admittance Ycbetween the amplifier inputs cause one of the biggest sources of the measurement uncertainty. This uncertainty (δΖ) strongly limits the measurements of the high impedances on high frequencies. δΖ is described by the equation:

δΖ=YcZ0/1+KE15

If K » 1, we can write:

δZYcZ0/KE16

Here, the values Ycand K are the disturbing factors. The quotient of the Ycand K can be considered as the sole source of the uncertainty. Let us provide the multiplicative variation of the gain Kof the amplifier A. To vary K on ratio α1, the divider Dvwith transfer coefficient 1 or α1 (Figure 5) is used. After this variation, MC measures the additional voltage U0v.

The system of three equations describes the measurements of the voltages Ux, Uo and Uov.

Ux=IxZx;U01YcZ0/K=IxZ0;U01YcZ0/K=IxZ0E17

Solution of this system gets the following formula (18):

Zx/Z0=Ux1δUα1/1α1/U0E18

where δU=1U0/U0v

Analysis of the formula (18) shows that the uncertainty of the variation calibration has minimal if α1=0.5. Then:

Zx/Z0=Ux1δU/U0E19

Formula (19) shows that the ratio Zx/Z0 does not depend on the quotient of the Ycand K.

But here increases component of the uncertainty, caused by the increased number of measurements. VV measures quadrature components a and b of three voltages: Ux, Uo and U0v. Let us suppose that effective input noise of the VV in all these measurement has the same value Δ and the results of measurement are not correlated. In this case, the following formulas are justified:

Ux=ax+Δ+jbx+Δ;U0=a0+Δ+jb0+Δ;U0v=a0v+Δ+jbx+ΔE20

Let us substitute formula (20) in (14) and (19). It gets the following formulas for two cases:

Without variational calibration:

δm2δnandΔa2δnE21

With variational calibration:

δm5δnanda2δnE22

where δmand Δaare the multiplicative and additive uncertainties caused by the relative noise δnof the VV.

Formulas (21) and (22) show that the additive uncertainty acaused by the relative noise (δn=Δ/U0) in both cases is the same. But these formulas also show that due to the variational calibration, the multiplicative random uncertainty δmincreases 1.6 times.

Calculation of the uncertainty by the formula (16) has the truncation error δtcaused by inequality K » 1 δt=Z0Yc/K. This error sharply increases when K on high frequencies is low, so that calibration practically does not work when K → 1. If amplifier gain K is so low, we cannot consider value Yc/K as the sole source of the uncertainty. As a result, we have to provide two separate variations: multiplicative variation of the gain K and additive variation of the admittance Yc (using variational admittance Yv and switcher Sv). DVV measures sequentially voltages Ux,U0and U0',U0''after multiplicative variation of the gain K and additive variation of the admittance Yc.

System of three equations describes these four measurements:

Ux/U0=Zx/Z01+YcZ0/1+KUx/U0=Zx/Z01+YcZ0/1+α1KUx/U0=Zx/Z01+Yc+YνZ0/1+KE23

Solution of the system (23) gets following two equations:

YcZ0=A'1α1K+1K+1/K1α1aK2+bK+c=0E24

here: a=[(1+α1)α1(A'1)](A''1),b=(YvZo+A')A''A',c=(A'1)(A''1),A=U0'/U0,A''=U0'/U0

Solution of the Eqs. (24) and substitution of these results in (15) gets the accurate results of measurement which absolutely does not depend on the values Ycand K.

The described approach could be used for the accurate calibration of any amplifier with positive or negative gain, followers, gyrators, and so on. It could be used for calibration of any control system as well.

## 3. Experimental results

The earlier described approach was used in digibridge MNS1200. This digibridge was developed for Siberian Institute of Metrology (Novosibirsk), to be used in working inductance standard. Its short specification is as follows.

MNS1200 operates in frequency range of DC to 1 MHz.

Frequency set discreteness 2 × 10−5.

Capacitance range of measurement (F) 10−17–105.

Resistance range of measurement (R) 10−6–1014.

Inductance range of measurement (H) 10−12–1010.

Dissipation factor tgδ (tgφ) 10−6–1.0.

Main uncertainty (ppm) 10.

Sensitivity (ppm) 0.5

Inner standard instability (24 hours, ppm) ± 2.

Weight (kg) 4

MNS1200 appearance is shown in Figure 6.

Instability of the MNS1200 inner standard can achieve 10−4 in a long period of time. To get maximal accuracy, MNS1200 can be calibrated by arbitrary R,L,C outer standard. In this case, uncertainty of measurement depends on short-time stability of inner standards. Results of the 24-hour 1 Ohm standard measurements are shown in Figure 7.

### 3.1. Application of the VM in transformer bridge

Accurate comparison and unit dissemination of the impedance parameters are provided using many different, very complicated manual bridges with numerous different standards. The main world-renowned laboratories (BIPM, NIST, NML, NPL, PTB, VNIIM, etc.) in developed countries have their own primary standards, based on the calculable capacitor [13, 14] and the appropriate transformer bridges [15, 16], on the quantum hall resistance [17] and the appropriate bridges [18, 19] and very accurate quadrature transformer bridges for comparison of different impedance parameters [20, 21], that have original constructions. All these bridges contain complicated set of devices and have long and intricate handle balancing processes. In addition, these bridges and standards are of different kinds and are located in various laboratories. The process of calibration and traceability is, therefore, complicated and very expensive. Uncertainty of the measurement of these bridges achieves 10−8–10−9. It makes them an excellent instrument for fundamental investigations.

For practical needs of the metrologic calibration, it is enough to provide measurements with uncertainty about 10−6. In this case, the equipment have to be universal, to compare arbitrary standards, to have low cost and weight and to be transportable. The complex of bridges described later satisfies these demands. Complex consists of autotransformer and quadrature bridges. Both of them are based on the variational calibration. Autotransformer bridge provides unit transfers in the whole range of the impedance of the C,L,R standards. Quadrature bridge provides cross transfers of the units. Last bridge is described in [22, 23].

This chapter describes the part of the results of this project, covering the development of the transformer bridge-comparators which transfer units of the resistance, inductance, capacitance and dissipation factor in a whole range of measurements and reciprocal transfer of any units. Balance and calibration of these bridges are based on the variational method.

#### 3.1.1. Autotransformer bridge: description and analysis

Early autotransformer bridges were described in [24, 25]. These bridges have been widely used up to now [15, 16]. To eliminate the influence of the cable impedance (yoke) on the results of measurement, double autotransformer bridges are used [3, 5]. The wide-range double autotransformer bridge contains two inductive dividers, simultaneously controlled for bridge balance. For accurate measurements, these inductive dividers usually are of a two-stage design at least. Every stage of these inductive dividers [26] consists of a lot of turns and appropriate complicate switchers. They have to have multidigit capacity (up to seven or eight digits). This quite complicates the bridge.

Development of the variational bridge has to solve two problems:

• to eliminate the Yoke (Zn) influence on the results of measurement without using the double autotransformer bridge;

• to decrease sharply the number of the autotransformer divider decades without loss in the accuracy of measurement.

The simplified measuring circuit of the automatic variational bridge (PICS) [27], which solves these problems, is shown in Figure 8.

The bridge consists of the supply unit (the generator G connected to the voltage transformer TV), the main autotransformer AT and the variationally balanced 90° phase shifter [28], which is calibrated through calibration circuit CC. The vector voltmeter VV (through the preamplifier PA and switchers S1 and S2) measures the bridge (U1, U2) and the calibration circuit CC (Uc) unbalances the signals. The differential voltage follower 1:1 compensates the voltage drop Un on the cable impedance Zn. The microcontroller μC transfers the results of the VV measurements to the personal computer PC and controls the bridge balance and calibration of the phase shifter 90°. The autotransformer AT Carries on its core windings m2, m1c and m1k. These windings are used to balance the bridge by the main (m1c) and secondary (m1k) parameters. The standards to be compared Z1 and Z2 are connected serially by the cable (yoke) and by their high potential ports, to voltage transformer TV and to the windings m1c and m2 of the autotransformer AT.

The output of the 90° phase shifter is connected in series with the winding m1c to create the balance winding m1=m1c+jm1k.

The drop of the voltage Un acts on the impedance Zn of the cable which connects Z1 and Z2. This voltage is applied to the input of the differential voltage follower 1:1.

The two-channel VV has two digital synchronous demodulators, proper LF digital filters and Σ-Δ ADC. It simultaneously measures two orthogonal components of the bridge unbalance signals. This voltmeter has high selectivity (equivalent Q-factor is higher than 105). Its integral nonlinearity is better than 10−4 and relative sensitivity is better than 10−5. The VV is calibrated automatically and periodically by variational algorithm, described in [29].

On the low impedance ranges, the drop Un of the voltage on the cable impedance increases. This increases the uncertainty of the bridge unbalance measurement. To decrease this effect, the voltage follower 1:1 is used. This follower places the named drop of the voltage between low potential pins of the windings m1 and m2. It decreases the effective cable impedance from Zn to the equivalent value Zne = Znδ, where δ is the uncertainty of the transfer coefficient of the voltage follower.

To decrease the number of the decades of the autotransformer divider and eliminate the influence of the Zn on the results of measurement, the bridge operates in a non-fully balance mode and use twice variational balance [27].

In compliance with developed variational algorithm, VV measures sequentially the bridge unbalance signals U1 and U2. After that, μC varies the turns of the winding m1 on ∆mv and VV measures the variational signal U2v.

The system of Eqs. (30) describes these three measurements:

U0Z1/ZcU01Zn1+δ/Zcm1/m1+m2U1=0U01Zn1+δ/Ζcm2/m1+m2+U0Z2/Zc+U2=0U01Zn1+δ/Ζcm2/m1+m2+Δmv+U0Z2/Zc+U2v=0E25

where Zc = Z1 + Z2 + Zn, and δis the uncertainty of the voltage follower 1:1, U0is the supply voltage.

The formula (26) gives the solution of the system (25):

δZ=δv2m1+m2m2C+m1m2m1+m2D/1+C+DδvE26

where

C=U2+U1/U2vU2;D=U2U1/U2vU2;δv=δm/1+δm;δm=Δmv/m1+m2

μC uses the results of the calculation of the bridge unbalance δZcby described algorithm in two stages:

• in the first stage, μC makes quick, automatic balance of the bridge on the four high-order decades (balance stage);

• in the second stage, μC increases the sensitivity of the voltmeter VV on 104 and decreases the value of the variation ∆mv of the m1 turns in the same ratio. Then, μC repeats the measurements by described algorithm. Results of these measurements and calculations by formula (26) determine the balance point coordinates and find the impedance ratio:

Z1Z2=m1m2δZE27

The final result is given in 8.5 digits.

The bridge balance and data processing by described variational algorithm reduce the number of the autotransformer dividers to only one and sharply (twice) reduce the number of the digits of this divider.

The 90° phase shifter and the calibration circuit CC do not contain accurate internal standards of capacitance or resistance. To get good accuracy, we use the special phase shifter calibration procedure based on the variational method. Simplified structure of this phase shifter is shown in Figure 9.

Phase shifter consists of serially connected inverter I and proper phase shifter PS. Firstly, calibrating circuit (resistors R1 and R2) and switchers S1 and S2 are used to calibrate inverter I. Secondly, calibrating circuit (resistor R1 and capacitor C1) and switchers S3 and S4 are used to calibrate the phase shifter PS. Vector voltmeter VV, through switcher S5 measures unbalance signals of the first or second calibration circuits and translates the results of measurements to microcontroller μC. Finally, one controls all calibration procedure and calculates PS real transfer coefficient.

Calibration procedure consists of two stages.

## 4. Calibration of the inverter I

To calibrate the inverter, the VV measures three signals of the calibration circuit R1–R2:

• The initial output signal of the calibration circuit Ui1;

• The signal Ui2 after the variation of the inverter transfer coefficient on the value δiv;

• The signal Ui3 after the inversion of the connection of the calibration circuit between the input and output of the inverter I by the switchers S1 and S2.

Complex of these signals is described by proper system of equations. Solution of this system (formula 38) gets the accurate deviation δiof the inverter transfer coefficient from its nominal value “1.”

δi=δia1+δkiaE28

where.

δiaδiv2Ui3+Ui1Ui2Ui1; δkiaδiv2Ui3Ui1Ui2Ui1; δiaand δkiaare the approximate values of the transfer coefficients of the inverter I and calibration circuit R1-R2.

## 5. Calibration of the phase shifter PS

To calibrate the phase shifter PS, the VV measures three signals of the calibration circuit R3-C1:

• The initial output signal Up1 of the calibration circuit, when calibration circuit is connected between input and output of the phase shifter;

• The signal Up2 after the variation of the phase shifter PS transfer coefficient in the value δpv;

• The signal Up3 after the inversion of the calibration circuit and connection of this circuit between the input of the inverter I and output of the phase shifter PS by the switchers S1 and S2.

Complex of these signals is described by proper system of equations. Solution of this system (formula (29)) gets the accurate deviation δpof the phase shifter PS transfer coefficient from its nominal value “j”:

δp=δpa1+δkpaE29

where:

δpaδpv2jUp3+Up1Up2Up1δi211+δiandδkpaδpv2jUp3Up1Up2Up1δi211+δi

δpaand δpkaare the approximate values of the transfer coefficients of the inverter PS and calibration circuit, respectively.

After the calibration procedure, we know the real value of the phase shifter transfer coefficient with an uncertainty better than 1–3 ppm. μC makes this calibration procedure automatically at least every hour.

### 5.1. Experimental results

All results of the theoretical investigations shown earlier were used to develop the comparator PICS.

PICS very short specification is given as follows.

Short PICS Specification.

PICS operates on frequencies 1.00 and 1.59 kHz.

Frequency set discreteness 5 × 10−5.

Capacitance range of measurement (F) 10−19–10−3.

Resistance range of measurement (R) 10−7–108.

Inductance range of measurement (H) 10−12–103.

Dissipation factor tgδ (tgφ) 10−6–1.0.

Main uncertainty (ppm) 1.0.

Sensitivity (ppm) 0.02–0.05

Weight (kg) 5

PICS was tested in USA (NIST) and Russia (VNIIM), in Germany (PTB) and Poland (GUM), in Ukraine (Ukrmetrteststandard) and Byalorussia (Center of metrology).

Some results of these tests are shown in Figure 10.

Appearance of the PICS, together with intermediary thermostated standards, is shown in Figure 11.

## 6. Conclusion

Variational calibration sharply increases the accuracy of measurement. In case of variation correction, for precision measurements, we can use simple and cheap measuring circuits with rather high uncertainty. Variational calibration diminishes the uncertainty of such circuits on thousands or even more times. It does not need too accurate variational standards. Time and space clustering in significant measure overcomes disadvantages of this calibration—increasing the time of measurement. Experimental investigations of the comparator PICS have shown that uncertainty of measurement on main ranges is lower than 10−6 and sensitivity is better than 10−7–10−8. Variational calibration also decreases the weight and cost of the accurate equipment.

## Acknowledgments

The author is grateful to Dr. H. Bachmair, Dr. J. Melcher and Dr. M. Klonz (PTB), to Dr. A. Koffman, Dr. J. Kinnard and Dr. Y. Wang (NIST), to Dr. A. Tarlowski (GUM) for their constant support and very useful advice during the project development, to Dr. H. Hall for his very helpful criticism and advice during paper consideration. I would like to specially acknowledge my teacher F. B. Grinevich and colleagues A. Lameko and D. Surdu, who have spent a great part of their life realizing variational ideas.

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Michael Surdu (August 1st 2018). Variational Calibration, Metrology, Anil, IntechOpen, DOI: 10.5772/intechopen.74220. Available from:

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Edited by Anil Akdogan

First chapter

#### Introductory Chapter: Mass Production and Industry 4.0

By Anil Akdogan and Ali Serdar Vanli

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