Open access peer-reviewed chapter

# Scaling in Magnetic Materials

By Krzysztof Z. Sokalski, Barbara Ślusarek and Jan Szczygłowski

Submitted: October 14th 2015Reviewed: March 23rd 2016Published: August 24th 2016

DOI: 10.5772/63285

## Abstract

The chapter presents applications of the scaling in several problems of magnetic materials. Soft magnetic materials (SMMs) and soft magnetic composites (SMCs) are considered. Application of scaling in investigations of problems, such as power losses, losses separation, data collapse of the losses characteristics and modelling of the magnetic hysteresis, is presented. The symmetry group generated by scaling and gauge transformations enables us to introduce the classification of the hysteresis loops with respect to the equivalence classes. SMC materials require special treatment in the production process. Therefore, algorithms for optimization of the power losses are created. The algorithm for optimization processes is based on the scaling and the notion of the pseudo-equation of state. The scaling makes modelling and calculations easy; however, the data must obey the scaling. Checking procedure of statistical data to this respect is presented.

### Keywords

• magnetic materials
• hysteresis loop
• power losses
• losses separation
• scaling
• gauge

## 1. Introduction

The notion of scaling describes invariance of various phenomena and their mathematical models with respect to a change of scale. Let us take into account the simplest mathematical model revealing such behaviour:

y=AxαE1

where α and A are the constants of model. Such functions appear in mathematical modelling in physics, mathematics, biology, economics and engineering. In this section, we consider data of classical gas. By simple calculation, we will prove that these data are self-similar. Let us change the scale of the both variables x and y with respect to λ > 0 multiplier.

x'=λβx,y'=λγy.E2

Substituting (2)(1) we obtain:

y=Axα,E3

where β and γ are scaling exponents and A′ = λγαβ A is the model constant in new scale. (1)(3) reveal that the phenomenon described by the model (1) is self-similar. This means that the phenomenon reproduces itself on different scales. In achieving the property of self-similarity, an important role plays dimensional analysis. Its idea is very simple: physical laws cannot depend on an arbitrary choice of basic units of measurement . Set of all transformations (2) and multiplication constitutes =(+,·)group. In the next section, we will consider self-similar model of hysteresis loop. Extension of (2) to the two parameters group is necessary to this respect. Let us extend (1) to non-homogenous form:

y=Axα+c,E4

The full symmetry of (4) consists of the two transformations, λ scaling and χ gauge transformation:

y=A(λx)α+c+χ.E5

where χϵis additive gauge operation which constitutes additive group =(,+).Therefore, the full symmetry of (5) consists of the following direct product: . However, the symmetry of the hysteresis loop will occur to be semi-direct product.

In this chapter, we will consider more advanced function and then the models (1) and (4). Therefore, we will need definition of homogenous function in general sense  which has played crucial role in the all achievements presented in this chapter. Let f(x1, x2, … xn) be a function of n variables. If (α0,α1,α2,αn)ϵn+1such that λϵ+, the following relation holds:

λα0f(x1,x2,xn)=f(λα1x1,λα2x2,λαnxn).E6

Then, f (x1, x2, … xn) is homogenous function in general sense. Based on the measurement data of classical gas presented in Table 1, we present simple application of this notion. We assume that the phenomena are represented by measurement data which satisfy certain relation called law. Let us assume that searched on phenomenon have a form of the homogenous function in general sense:

λaρ(T,p)=ρ(λbT,λgp).E7

ρ[mol·m-3]T[K]p[Pa]
0.096500400
0.090515385
0.084530370
0.078545355
0.073560340
0.068575325
0.063590310
0.059605295
0.054620280
0.050635265
0.046650250

### Table 1.

Measurement data of classical gas.

where ρ, T and p are gas density, temperature and pressure, respectively. Coefficients a, b and c are the scaling exponents. Since (7) holds for each value of λ, we are free to substitute the following expression λ = T−1/b and get the following relation:

Ta/bρ(T,p)=ρ(1,Tg/bp).E8

Introducing new symbols for the scaling exponents: α=ab,γ=gbwe derive the following equation of state:

Tαρ=ATγpE9

where the right-hand side of (8) was approximated by linear function, A is an expansion’s coefficient. In the next sections of this chapter, we will use the Maclaurin expansion beyond the linear term as a way for creation of scaling function. Equation (9) depends on the one effective exponent δ = γα:

ρ(T,p)=ApTδ.E10

where the model constants A and δ have to be determined from the experimental data of Table 1. Using formula (10) and Table 1 we have created error function Chi2 which was minimized by the SOLVER program of the Excel package. The obtained results are as follows: A = 0.121 (mol K J−1) and δ = 1.002 (−). Note that A−1 = 8.22 (mol−1 K−1J) reveals an approximation of the gas constant. Mentioned and illustrated above methodology for applications of the scaling and the gauge transformations will be applied to the following problems: self-similarity of hysteresis, self-similarity of total loss in SMM, multi-scaling of core losses in SMM, optimization of total loss in SMC and scaling conception of losses separation.

## 2. Self-similar model of hysteresis loop

The goal of the present section is to describe the self-similar mathematical model of hysteresis loop which enables us to express its self-similarity by the homogeneous function in general sense. Derivation of the model based on the well-known properties of tanh(⋅) suits for model of initial magnetization function . It describes properly the saturation for both asymptotic values of the magnetic field H → ±∞, as well as and the behaviour of magnetization in the neighbourhood of origin. However, this is too rigid for scaling. We make tanh(⋅) to be a softer by making the base of the natural logarithm free parameters :

tanh(x)>tanH(a,b,c,d;x)=axbxcx+dx.E11

where the bases have to satisfy the following conditions: a > 1, b > 1, c > 1, d > 1. These conditions guarantee correctness of the model; however, a little deviations from the mentioned constrains are possible.

First, we write down the model expression for initial magnetization curve:

MP(X,ε)=M0P(X,ε);X𝜖[0,Xmax]E12

where M0 is magnetization corresponding to saturation expressed in tesla: [T], X=Hh, where H is magnetic field, and h is a parameter of the magnetic field dimension (A m−1) to be determined. Function P(X, ε) is of the following form:

P(X,ε)=aXεbX+εcXεdX+εE13

where ε is modelling parameter related to θ, where εϵ[θ2,+θ2]. Let the upper and the lower branches of the hysteresis loop are of the following forms:

MF(X,θ)=M0F(X,θ);MG(X,θ)=M0G(X,θ).E14

where

F(X,θ)=aX+θbXθcX+θdXθG(X,θ)=aXθbX+θcXθdX+θ.E15

Let us consider for illustration the following symmetric example: a = b = c = d = 4 and θ = 1.3, ε = 0, M0 = 1 (See Figure 1). Figure 1.A model of nucleation-type hysteresis constructed with functions F, P and G according to (12)–(15).

Due to the asymptotic properties of magnetization, the functions F(X, θ) and G(X, θ) have to possess the same asymptotic properties. As we have mentioned, these components get equal values for H → ±∞. However, due to the uncertainty of measured magnitudes, it is possible to accept the saturation points at X = Xmin and X = Xmax being the end points of the hysteresis loop. Therefore, the modelling process has to ensure that the initial function satisfies the following constrain:

|F(Xmax,θ)G(Xmax,θ)||𝜓|E16

where |ψ|=supX|MF(X,θ)MG(X,θ)|M0is dimensionless measure of uncertainty corresponding to |MF(X)MG(X)|.

The scaling in space of loops is performed by scaling each loop’s component (13), (14), (15) and (16). For simplicity of further investigations, we consider simplified symmetric model, where all the bases of tanH( ) are equal:

MF(X,θ)M0=(a)X+θ(a)Xθ(a)X+θ+(a)XθE17
MG(X,θ)M0=(a)Xθ(a)X+θ(a)Xθ+(a)X+θE18
MP(X,ε)M0=(a)X+ε(a)Xε(a)X+ε+(a)XεE19

Let us perform scaling on (17) and (18). Since exponents are dimensionless, the scaling on this level cannot be supported by dimension analysis. However, we are able to scale the following magnitudes a, MF(X, θ), MG(X, θ), MP(X, θ), and to prove the following theorem:

For the symmetric model (17)(19), the hysteresis loop is invariant with respect to scaling and gauge transformation . Following definition of the homogeneous function in general sense (6), we write down the scaled form of the hysteresis loop:

MF(X,θ)M0λν=(λαa)X+θaχ(λαa)Xθaχ(λαa)X+θaχ+(λαa)Xθaχ,E20
MG(X,θ)M0λν=(λαa)Xθaχ(λαa)X+θaχ(λαa)Xθaχ+(λαa)X+θaχ,E21

where exponentials aχ and aχ represent action of the gauge transformation. This formal trick guarantees proper order of actions: the first has to be performed scaling than after that gauge transformation. According to the assumption just above (6), we are free to make the following substitution:

λα=ap1E22

where . Substituting (22) leads to the following forms of (20) and (21):

MF(X,θ)M0an=(a)p(X+θ)+χ(a)p(Xθ)χ(a)p(X+θ)+χ+(a)p(Xθ)χE23
MG(X,θ)M0an=(a)p(Xθ)+χ(a)p(X+θ)χ(a)p(Xθ)+χ+(a)p(X+θ)χ.E24

where for abbreviation, we introduce n=να(p1). Introducing the following new variables:

M0=anM0,X=pX+χ,θ=pθ,E25

we derive (17) and (18), which proves the considered thesis. The initial magnetization curve (19) is invariant with respect to scaling and gauge transformation as well. The proof goes the same way as for (17) and (18). Therefore, we can formulate conclusion that the presented model of hysteresis loop is self-similar. Below in Figures 24, we present some examples of the hysteresis loops which may suggest how to apply the scaling and gauge transformation for modelling of hysteresis phenomena. Figure 3.Magnetic hysteresis family for a=4,χ=0,n=1,θ=1.3,να=1. Figure 4.Magnetic hysteresis family for the following values of the model and scaling parameters: (a) a=4, θ=3, p=14, vα=−0.18,χ=0,(b) a=4,θ=2,p=13,vα=−0.18,χ=0, (c)a=4,θ=1.3,χ=0,(b) θ=2, p=13,vα=−0.18,χ=0.

Figure 2 presents how the pure gauge transformations generate a displacement of transformed loops along the horizontal axis. Figure 3 presents compression of loops along the vertical axis under the scaling. Finally, Figure 4 presents the loop’s family for large value of the scaling parameter p. Each element of this set resembles the Preisach hysteron [6, 7].

Multi-scaling of hysteresis loop. The derived above mathematical model of the hysteresis loop is not full. There is need to extend considered model with respect to frequency, pick of induction and temperature. As we have shown the loop’s model is self-similar with respect to scaling of the following magnitudes X, M0 and θ, these are as follows: dimensionless magnetic field, amplitude of magnetization and loop’s closing parameter, respectively. By introducing new independent variables, we introduce new scales and corresponding new scaling parameters . We have shown in [8, 9] that it is always possible to introduce a new characteristic scale; however, one must investigate whether the considered system possesses corresponding symmetry. This can be known only from investigations of the measurement data. In the considered model, there are two places where the new variables can be implemented. These are base of the tanH() function and the loop’s closing parameter θ. There are many possible combinations for configurations of the new variables in presented model which can be applied:

(i)[Bmβ'a(fBmα',TBmγ);Bmβ'θ(fBmα',TBmγ)];(ii)[Bmβa(fBmα',TBmγ);Bmβ'θ()];(iii)[Bmβ'a(fBmα');θ()].E25a

The list (25a) is not closed and can be extended as needed. We assume that a(f, Bm, T) and θ (f, Bm, T) are homogenous functions in general sense. To simplify considerations, we chose for illustration the temperature less model (iii), where θ(−) is a constant. For the model of the function a(fBmα), we chose the square polynomial:

a=Bmβ(Γ1fBmα+Γ2(fBmα)2)E25b

where α,β,Γ1,Γ2are model constants to be calculated from the measurement data, whereas the Bm pick of induction is correlated with Xmin and Xmax. Formulae (25b), (14) and (15) constitute frequency- and pick of induction-dependent loop model.

Equivalence classes and partitioning . Transformation formulae (25) enable us to investigate algebraic structure of all the transformations which are composed of scaling and gauge transformation. Therefore, the whole set of p and the multiplication constitute Gp={\0, · }group. Moreover, ∀a > 0 and vα0, the following expression a(1p)ναrepresents an infinite number of groups being isomorphic to . Gauge transformations χϵand the addition constitute group. Each of revealed group possesses the own representation space. group operates in the spaces generated by X, θ and M0 and group operates in the space spanned by X variable. The considered model of loop reveals a combination of and which operates in space generated by (X, θ) pair. Therefore, total symmetry of the considered model can be presented in the following matrix representation (26):

[p000a(1p)να000p][XM0θ]+[χ00]=[XM0θ0]E26

Therefore, the total symmetry of the considered group has got the structure of the following semi-direct product where p=a(1p)ναrepresents isomorphic mapping . Let Vh be space of the all hysteresis’ models represented by (14) and (15). Group element is automorphism in Vh if yields . Set of the all automorphisms GAconstitutes automorphism group, where Let us distinguish the loop v1=[X1M01θ1]Vh, and relate v1 with v2:

v1v2E26a

where ℛ means the binary relation given by (26).

Definition:

Equivalence binary relation on a set V(h) is a relation, which is reflexive, symmetric and transitive . Due to the group structure of (26a) satisfies these conditions and ℛ is equivalence relation.

Let ℛ be an equivalence relation on Vh, then Ev1Vh containing all elements v2Vh satisfying (26a) is called the equivalence class of v1. The sets Evi are pairwise disjoint, that is EviEvj=if vivj. Union of the all equivalence classes is the Vh space: viEvi=Vh. What practical use one may have from equivalence relations and partitioning. Let us assume the following v1v2relation, and then there exists a group element which relates both loops means that they are equivalent. However, in the opposite case, the two loops do not belong to a common class and then they are relevantly different from the algebra point of view.

## 3. Losses scaling in soft magnetic materials

Density of the total power losses in magnetic materials under variable magnetic field is due to eddy currents generated in the material. These may be generated for various scales of dimensions: currents caused by Barkhausen jumps, what leads to a dependence Phys(B1.6f), currents around moving domain walls Pexc(Bf)32 and currents in the whole material volume Pclas(Bf)2. All of the aforementioned dependencies obey a power law, however, with a diverse value of exponents . Therefore, one cannot talk about universality of the presented above formulae. However, certain universality of the power losses data of soft magnetic materials has been derived by applying the scaling. The proposed approach has been based on assumption that the density of the total power loss in soft magnetic materials was self-similar like intermittency of fully developed turbulent flow . Moreover, using simple model of hysteresis loop (14), (15) and assuming semi-static conditions, we derive the following formula for the total power loss :

Ptot=fμ0M0hanln((a2(pθ+pXmax+χ)+1)(a2(pXmax+χ)+a2pθ)(a2(pXmin+χ)+a2pθ)(a2(pθ+pXmin+χ)+1))(pln(a))1.E26b

In case of the symmetric extrema of magnetic field Xmin = −Xmax, (26b) gets the following form:

Ptot=4θfμ0M0hanE26c

where a,n=να(p1),h=HX,θand M0 are the hysteresis loop parameters and μ0 is the permeability of free space.

According to (26c), the formula for Ptot is monomial which is always self-similar mathematical expression. This theoretical result confirms experimental observations concerning homogeneity of Ptot in soft magnetic materials.

Let us assume that the density of the total power losses is homogenous function in general sense (6). Let Ptot (f, Bm) be density of the total power losses, where f and Bm are frequency and the pick of magnetic induction of flux waveform. Applying (6) for the two independent variables, we derive the most general form for Ptot:

Ptot(f,Bm)=BmβF(Bmαf),E27

where α and β are scaling exponents and F(⋅) is an arbitrary function. These three unknown magnitudes have to be determined from experimental data. As the simplest approach to estimation of F(⋅), we have applied the Maclaurin expansion of (27):

Ptot(f,Bm)=Bmβ(Γ(1)(Bmαf)+Γ(2)(Bmαf)2).E28

where Γ(k)=1k!Γ(k)(0). Since the total losses vanish for f = 0 or for Bm = 0, the constant term of expansion (28) equals zero.

### 3.1. Measurement data

The measurement of density of total power losses was carried out following the IEC Standards (60404-2, 60404-6). During measurements, the shape factor of secondary voltage was equal to 1.111± per cent. Extended uncertainty of obtained measurements was equal to about 0.5%. The measurements covered the three following classes of soft magnetic materials:

• Crystalline materials;

• Amorphous alloys, Co-based and Fe-based; and

• Nanocrystalline alloy.

Density of total power losses was measured as a function of the maximum induction Bm ∈ [0.1](T), 1.8(T)] at fixed values of f ≤ 400 (Hz). Samples of conventional crystalline materials were strips, whereas the remaining ones had the shape of cylinder.

### 3.2. Estimation of expansion parameters (28) from measurement data

Magnetic materialsα(−)β(−)Γ(1)(m2T(αβ)/s2)Γ(2)(m2T(2αβ)/s)
GO—3% Si-Fe−2.16 −1.19 12.78×10−337.68×10−6
Co71.5Fe2.5Mn2Mo1Si9B14−1.55−0.352.88×10−31.90×10−6
Fe73.5Cu1Nb3Si13.5B9−1.81−0.700.17×10−30.71×10−6

### Table 2.

Values of scaling exponents α, β and values of amplitudes Γ(k).

Firstly, the initial values of exponents α, β and amplitudes Γ(k) were assumed and differences between all measurement values of density of total power losses and values of density of total power losses obtained from expansion (28) were calculated. Next, the Chi2 function was optimized. Constraint of normal distribution of error was applied. Results of optimization for exponents α, β and amplitudes Γ(k) for chosen magnetic materials are given in Table 2.

The results, that is scaled values of the measurement data and the values obtained from the mathematical model, for the chosen magnetic materials, are shown in Figures 57, in the PtotBmβ,fBmαcoordinates system. Based on the all results concerning the density of total power losses, the universal relationship between the scaling exponents α and β was stated. This relation is of the following form :

β=1.35α+1.75,E29

See also Figure 8. The origin of the relationship in (29) will be subject of further relations. Figure 5.A comparison of measurement data of total density of power losses Ptot (markers) and values obtained from the scaling theory (solid line) for Co-based amorphous alloy Co71.5Fe2.5Mn2Mo1Si9B14. Figure 6.A comparison of measurement data of total density of power losses Ptot (markers) and values obtained from the scaling theory (solid line) for nanocrystalline alloy Fe73.5Cu1Nb3Si13.5B9. Figure 7.A comparison of measurement data for total density of power losses Ptot (markers) and values obtained from the scaling theory (solid line) for grain-oriented silicon steel 3% Si-Fe. Figure 8.The universal relationship of the scaling exponents α and β. Markers correspond to estimations from experimental data, and continuous line corresponds to (29).

The three achievements resulting from scaling should be emphasized. The first one is a satisfactory agreement between the measurement data and the theoretical description. The second one is relation (29), which establishes the universal linear relationship between the scaling exponents and decreases the number of free parameters. The third achievement consists in revealing the data collapse. Figures 57 are drawn in PtotBmβ,fBmαcoordinates system and present the continuous sets of the losses characteristics of different values of Bmcollapsed just to a single curve. This effect is called “a single-sample data collapse” Reversible procedure (PtotBmβ,fBmα)(Ptot,f)splits the collapsed curves to separate curves for different values of Bm. This effect will be demonstrated for more complicated case (see Figure 14). Therefore, the scaling can be also applied as method for a compression of data. All examples in Figures 57 present the single-sample data collapses. Having data for different materials and introducing for each of them are the following dimensionless magnitudes:

P˜tot=Γ(2)Γ(1)2PtotBmβf˜=Γ(2)Γ(1)fBmαE30

We obtain the multi-sample data collapse (see Figure 9). These results confirm the assumption of density of total power losses scaling. Applying these transformations to (28), we derive the dimensionless low for the density of power losses in soft magnetic materials:

P˜tot=f˜+f˜2E31 Figure 9.The multi-sample data collapse for total density of power losses P˜tot(markers) and values obtained from the scaling theory (solid line).

### 3.3. An application of the multi-sample data collapse

Mostly, the data collapse is applying as a tool for the detection of self-similarity. Here, we present a new application which solves problem of comparison measurements taken in different laboratories . In 1995, the leading European Laboratories busy with measurements of the electrical steel magnetic properties were trying to compare the measurement results of the power loss in electrical sheet steel under the conditions of rotating and alternating flux . Taking from  the idea of the inter-comparison of measurement data of the energy losses in soft magnetic materials, we perform such an inter-comparison with data taken in two laboratories [16, 18], however, under the conditions of axial and alternating flux. Self-similarity of the density power losses enables us to scale off the interference of the sample’s geometry and the material type from the dependence of power losses versus the pick of induction and magnetizing frequencies. This property of SMM allows comparing different measurement sets. Successively, this fact allows introducing an absolute measure of uncertainty characterizing the given measurement set. Therefore, the way for assessing the uncertainty contributions would not interfere with the abovementioned data comparison. Formula (30) suits very well to the mentioned above phenomena and constitute background for solution of the presented problem.

For inter-comparison, we have selected two sets of power losses data. The first one belongs to Yuan  and consists of the following three sets of data: S1=Fe76Mo2Si2P10C7.5B2.5,S2=Fe79.8Mo2.1Si2.1P8C6B2,S3=Fe80Mo1Si2P8C6B3. The samples were thin ribbons wound into toroids. For details concerning measurement methods, we refer readers to . On the basis of measured data, the parameters’ values of (28) have been estimated (see Table 3, after ).

Sampleα(−)β(−)Γ(1)(m2T(α−β)s−2)Γ(2)(m2T(2α−β)s−1)
S1−1.533−0.3196.744×10−31.322×10−6
S2−0.3641.2591.412×10−21.917×10−6
S3−0.5041.0699.11×10−33.389×10−6
P1−2.945−1.7762.90×10−34.60×10−6
P2−1.519−0.3752.53×10−36.79×10−6
P3−3.231−1.3653.22×10−41.95×10−7

### Table 3.

Scaling exponents and coefficients of (28).

*The data for S1, S2 and S3 have been kindly supplied by the authors of Yuan et al. .

The second set contains some of our results [15, 19] for the power losses in the following alloys: amorphous ribbon P1=Fe7.8Si13B9, Co-based amorphous alloy P2=Co71.5Fe2.5Mn2Mo1Si9B14 and nanocrystalline alloy P3=Fe73.5Cu1Nb3Si15.5B7.The corresponding scaling exponents α, β and the scaling coefficients Γ(1), Γ(2) are presented in Table 3.

Plotting P˜totversus f˜for the all considered samples (Figure 10), we confirm that the data collapse takes place for the selected samples. Figure 10.The data collapse for total power losses of compared materials.

Since all the magnitudes in (31) are dimensionless and the formula for P˜totis sample independent, we propose to introduce a measure of uncertainty characterizing the measurement set by the total distance of all empirical points from the scaling curve (31):

D=1Ni=1N(P˜totexp(f˜i)P˜totth(f˜i))2,E32

where P˜totexp,P˜totthare the power losses, measured and calculated from formula (31), f˜iis dimensionless frequency, where index i is running through the whole series of experimental data and N denotes length of the measured series. We consider the two sets of experimental data Sand ℙ corresponding to different LABs. Each set consists of the three series which correspond to different samples. To create effective measure of uncertainty characterizing measurement set of the given LAB, we calculate average measure Dav for the three samples belonging to either of two selected sets:

Dav2=i=13NiN1+N2+N3Di2.E33

Comparisons of uncertainty measures are presented in Table 4.

SampleNiDi2()Dav2()
S1481.64×10−58.11×10−3
S2407.42×10−3
S3321.29×10−4
P1489.23×10−56.53×10−3
P2472.05×10−5
P3491.53×10−5

### Table 4.

Comparisons of uncertainty measures.

Progress in modern technologies depends on the comprehensive knowledge of material properties under standard and non-standard conditions. However, an agreed standardized method does not exist, and the reproducibility of the different methods used in different laboratories is unknown. We are of the opinion that the reason of such situation is lacking of statistical method enabling the appropriate data’s inter-comparison. In this section, we have proposed a solution of this problem. As we have shown, the data collapse supplies method that enables us to introduce universal measure of uncertainty, which compares different experimental sets even based on different measurement methods. Therefore, the introduced method also can serve as a tool to compare measurement data obtained in different laboratories. The measure (33) expresses the total uncertainty characterizing the data set for the chosen range of dimensionless frequency f˜. There are four contributions to Dav resulting from the following: (1) uncertainty characterizing the measurement method and construction of the measurement set, (2) uncertainty of measurements of elementary magnitudes, (3) errors resulting from the approximation (28) and uncertainty of estimations of α, β, Γ(1) and Γ(2). The derived method is universal and can be applied to investigations of any phenomenon satisfying the self-similarity conditions.

## 4. Multi-scaling of core losses in soft magnetic materials

The application of soft magnetic materials in electronic devices requires knowledge of the losses under different excitation conditions: sinusoidal and non-sinusoidal flux waveforms of different shapes, with and without DC bias. Scaling theory allows the total power losses density to be derived in the form of a general homogeneous function, which depends on the peak to peak of the magnetic inductance ΔB, frequency f, DC bias HDC and temperature T:

Ptot=F(f,B,HDC,T)E34

The form of this function has been generated through the Maclaurin expansion with respect to scaled frequency. The parameters of the model consist of expansion coefficients, scaling exponents, parameters of DC bias mapping, parameters of temperature factor and tuning exponents. Values of these model parameters were estimated on the basis of measured data of total power density losses. However, influence of the DC bias on the self-similarity of measurement data was very relevant. In order to apply scaling to (34), the right-hand side has to be a homogeneous function in a general sense. This assumption has to be satisfied both by the experimental data and by the mathematical model. However, according to the results given in , Eq. (34) and measurement data are not uniform in the required sense when there is a DC bias. This problem has been solved by using the method invented by Van den Bossche and Valchev . Their method consists in mapping of magnetic field into a pseudo-magnetization by using tanh(⋅):

Ptot=F(f,ΔB,tanh(HDC·c0),T).E35

Following Bossche and Valchev, we have applied series of the mappings as expansion coefficients for modelling F(⋅,⋅,⋅,⋅) function of (35):

HDC[M0,M1,M2,M3]E36

where Mi=tanh(HDCci), where ci are expansion coefficients, to be determined from measurement data.Therefore, applying definition for the homogeneous function in general sense, we have formulated the following scaling hypothesis: {a,b,c,d,g}5:λ+yields: Ptot(λaf,λb(ΔB),λc[M0,M1,M2,M3],λdT)=λgPtot(f,ΔB,[M0,M1,M2,M3],T). Substituting the following λ = (ΔB)−1/b, we derive the most general form for Ptot which satisfies above hypothesis:

Ptot=(ΔB)βF(f(ΔB)α,[M0,M1,M2,M3](ΔB)γ,T(ΔB)δ).E37

where α=ab,β=gb,γ=cb,δ=dbare effective scaling exponents. F(⋅,⋅,⋅) is an arbitrary function of the three variables. Both the effective exponents and the F function have to be determined.

General formula (37) enables us to construct mathematical model which maps the four-dimensional space spanned by f, ΔB, DC bias and T into the one-dimensional Ptot space. In the first step, we separate the temperature factor Θ(⋅):

F(f(ΔB)α,[M0,M1,M2,M3](ΔB)γ,T(ΔB)δ)=Φ(f(ΔB)α,[M0,M1,M2,M3](ΔB)γ)Θ(T(ΔB)δ)E38

Let us assume that Φ(⋅,⋅) consists of two terms which need not be independent. However, the second one is HDC dependent in contrary to the first one. For both of them, we assume the Maclaurin expansions with respect to scaled frequency f/(ΔB)α, which is very much suited for the Bertotti decomposition. Moreover, the first term should describe losses for HDC → 0, whereas the second term must vanish for this condition. The resulting expression takes the following form:

Φ(f(ΔB)α,HDC)=Σi=14Γi(f(ΔB)α)i+Σi=03Γi+5(f(ΔB)α)itanh(HDCci)(ΔB)γ.E39

Since (39) has been created by the Maclaurin expansion, all series exponents are integers. However, it may be so that the best error’s minimum is obtained for fractional values of exponents. For this purposes, we introduce tuning exponents x and y:

Φ(f(ΔB)α,HDC)=Σi=14Γi(f(ΔB)α)i(1x)+Σi=03Γi+5(f(ΔB)α)(i+y)(1x)tanhtanh(HDCci)(ΔB)γ.E40

On the basis of some numerical test simulations, we have selected the following Padé approximant for Θ(⋅):

Θ=(𝜓0+θ(𝜓1+θ𝜓2)1+θ(𝜓3+θ𝜓4))1zE41

where θ=T+τΔBδis gauged and scaled temperature, T is measured temperature in °C, z is tuning parameter, and ψi are Padé approximant coefficients. After all improvements of F(⋅,⋅,⋅), the final form is still homogenous function in general sense (6).

In order to perform core loss measurements, the B-H loop measurement has been evaluated as the most suitable. This technique enables rapid measurement while retaining a good accuracy. The measurement set works in the following way: two windings are placed around the core under test. Taking into account the number of secondary winding turns and the effective core cross section, the secondary winding voltage V is integrated into the core flux density B. Next taking into account the number of primary winding turns and the effective magnetic path length of the core under test, the magnetic field strength H is calculated. Then, the total power losses per unit volume is the enclosed area of the B-H loop multiplied by the frequency f. The test system consists of a power stage, a power supply, an oscilloscope and a heating chamber. It is controlled by a MATLAB program running on a PC computer under Microsoft Windows. The power stage is capable of a maximum input voltage of 450 V, output current of 25 A and a switching frequency of up to 200 kHz. The B-H loop measurements have been performed for SIFERRIT. The rectangular voltage shape across the core and DC bias has been applied, while the duty cycle was 50%.

The tested core data were as follows:

1. - Material name: EPCOS N87

2. - Core shape: toroid R42

3. - Number of primary windings: 10

4. - Number of secondary windings: 5

5. - Magnetic path length [mm]: 354

6. - Cross section [mm2]: 840

The following factors influence the accuracy of measurements:

1. - Phase shift error of voltage and current <4%

2. - Equipment accuracy <5.6%

3. - Capacitive couplings negligible (capacitive currents are relatively lower compared to inductive currents)

4. - Temperature <4%.

AβδΓ1Γ2Γ3Γ4Γ5
−11.63−8.64−0.179−1.408739.51253.44238.50.123
Γ6Γ7Γ8c0c1c2c3γ
−30.97−51.87−4201.4−0.488−2.44E-02−0.1810.1650.00
Tψ1ψ2ψ3ψ4ψ5xy
7.77E-02−0.8992.39714.45−1.27E-010.2830.5260.289
z
4.84E-02

### Table 5.

The set of estimated model’s parameters of (37)(41).

TΔBfHDCPtotTΔBfHDCPtot
[°C][T][kHz][A/m][Wm−3][°C][T][kHz][A/m][Wm−3]
28.10.39518.6344064.328.10.391120.1464469.0
28.10.374160.6346332.428.30.351186.6516463.6
17.70.39827.8019452.117.80.398220.55510663.8
18.90.396235.58312745.818.50.377289.24016015.6
26.20.40056.57021131.326.40.4517.82023110.0
26.50.398533.23028057.327.10.386589.40035209.8
28.40.401105.89241549.028.60.4011017.47745257.9
28.80.4001031.82054650.929.70.3931073.96063821.6
30.80.38610105.00064632.128.40.49111.6946611.0
28.40.488124.2997196.028.40.451178.3908771.6
19.10.497210.12015234.119.20.496223.71816781.0
19.30.485254.63019235.919.80.475276.86020100.2
27.70.50258.92034634.827.40.503515.02036195.2
27.70.501521.50037496.628.60.496547.50041259.7
31.70.4991020.52071226.832.20.4941045.04076876.5
32.60.4871067.14080858.228.50.588114.42010042.9
28.70.561157.97011239.628.70.541178.08011255.7
29.10.580212.82019689.928.70.576254.36022043.0
30.10.592542.40052126.731.10.5991010.29092648.6
31.30.5951031.23096446.428.90.684122.05014150.5
28.10.389133.5075358.828.40.346191.0666376.4
18.20.386268.03415049.118.70.3672110.59016027.7
26.80.394558.80032614.327.50.386597.77935945.6
29.20.3961061.17262814.430.20.3871099.19064410.1
28.30.473154.3008296.528.50.443185.1008702.4
19.70.480268.36020073.320.20.469287.44020547.5
28.10.500531.42039530.231.50.499107.57065879.7
27.30.501515.03036194.328.50.58136.01010790.0
28.70.586233.49021002.230.20.616536.05054344.9
34.70.5861061.25096583.329.00.669141.33014417.5

### Table 6.

Selected 60 records of the measurement data of SIFERRIT N87. Figure 11.Projection of the measurement points and the scaling theory points (38)–(41) in ((fΔBα)(1−x),Ptot/ΔBβ) plane. Figure 12.Projection of the measurement points and the scaling theory points (38)–(41) in ((tan h(c1HDC), Ptot/ΔBβ) plane.

Some comments concerning temperature change/stabilization have to be done. For details of the applied measurement method and the errors of the relevant factors, we refer to [22, 24]. The parameter values of (37)(41) have been estimated by minimizing χ2 of our experimental data and using the simplex method of Nelder and Mead . The measurement series consists of 60 points (see Table 5). The standard deviation per point is equal to 15 Wm−3. Applying the formulae (37)(41) and the estimated parameter values (Table 6), we have drawn the three scatter plots given in Figures 1113, which compare estimated points those obtained through experimentation in the three projections, respectively. Note that in order to ensure numerical stability during the estimation process, the unit of frequency was set at 1 kHz, while other magnitudes were expressed in the SI unit system. Figure 13.Projection of the measurement points and the scaling theory points (38)–(41) in ((T + τ)/ΔBδ,Ptot/ΔBβ) plane.

Scaled variables Ptot/(ΔB)β and f/(ΔB)α are very convenient for the model parameter estimations. By using these variables, the number of independent variables is reduced. Also the collapsed form of power losses characteristic is very compact and easy to implement. However, for the purpose of designing of magnetic circuits, it is necessary to have the split characteristics which describe the physical magnitude Ptot versus the physical ones: T, f, HDC and ΔB. Note that formula (37) is suitable just for this task. Let us assume the characteristics family for the following values of the independent variables: T, f, HDC and T=30°C, HDC=7Am, ΔB={0.40.7}T, and f = ∈ {0.0 – 10.0}kHz. Using (37) and applying (38)(41) as well as Table 6, we derive the characteristics presented in Figure 14.

The efficiency of scaling in solving problems concerning power losses in soft magnetic material has already been confirmed in recent papers [15, 25]. However, this paper is the first one which presents an application of scaling in modelling the temperature dependence of the core losses. The presented method is universal, which means that it works for a wide spectrum of excitations and different soft magnetic materials. Moreover, the presented model formulae (37)(41) are not closed and can be adapted for a current problem by fitting the forms of both factors Φ and Θ. Ultimately, one must say that the degree of success achieved when applying the scaling depends on the property of the data. The data must obey the scaling. Figure 14.Family of the power losses characteristics Ptot versus frequency f derived for SIFERRIT N87 material for T=30°C,HDC=7Am.

## 5. Optimization of power losses in soft magnetic composites

Recently, novel concept of technological parameters’ optimization has been applied in soft magnetic composites (SMCs) by Ślusarek et al. . This concept is based on the assumption that power losses in SMC obey the scaling law. The efficiency of this approach has been confirmed in . The scaling is very useful tool due of the three reasons:

• It reduces number of independent variables f and Bm to the effective one f/Bmα,

• Determines general form of losses of power characteristic in a form of homogenous function in general sense, and

• Determines general form of losses of power characteristics in a form of different dimensions.

Therefore, applying concept of the homogenous function in general sense, we apply the following expansion:

PtotBmβ=(f/Bmα)(Γ1+f/Bmα(Γ2+f/Bmα(Γ3+f/BmαΓ4)))E42

Γn, α and β parameters have been estimated for different values of pressure and temperature . For the purpose of this paper, we take into account only one family of power losses characteristics which are presented in Figures 15 and 16. The corresponding estimated values of the model parameters are presented in Table 7. For all other details concerning SMC material and measurement data, we refer to . Now we are ready to formulate the goals of this section. Main goal is to describe minimization of the power losses in SMC by using model density of power losses (42) and corresponding values of the model parameters. From the first row of Table 7, we can see that dimensions of the Γn coefficients depend on the values of α and β exponents. Therefore, the power losses characteristics presented in Figures 15 and 16 are different dimensions. So, we have to answer the following question: Are we able to relate them in the optimization process which has been described in [9, 26]? Figure 15.Selection of the power losses characteristics Ptot/(Bm)α versus f/(Bm)α calculated according to (42) and Table 1 for Somaloy 500 , T = 500°C.

In this section, we show that if the considered characteristics obey the scaling, then the binary relation between them is invariant with respect to this transformation and comparison of two magnitudes of different dimensions has mathematical meaning. Reach measurement data of power losses in Somaloy 500 have been transformed into parameters of (42) versus hardening temperature and compaction pressure (Table 7) in . Information contained in this table enables us to infer about topological structure of set of the power losses characteristics and finally to construct pseudo-state equation for SMC and derive new algorithm for the best values of technological parameters.

Scaling of binary relations. Let the power losses characteristic has the form determined by the scaling (27). It is important to remain that α and β are defined by initial exponents a, b and c (see after formula (27)):

α=ab;β=cb.E43

Let us concentrate our attention at the point on the fBmαaxis of Figures 15 or 16:

fBmα=f1Bm1α1=f2Bm2α2=f3Bm3α3=f4Bm4α4.E44 Figure 16.Selection of the power losses characteristics Ptot/(Bm)α versus f/(Bm)α calculated according to (42) and Table 1 for Somaloy 500 .

Let us take into account the two characteristics and let us assume that

Ptot1Bm1β1>Ptot2Bm2β2.E45

TpαβΓ1Γ2Γ3Γ4
[°C][MPa][−][−][m2 s−2Tα−β][m2 s−1T2α−β][m2T3α−β][m2 sT4α−β]
500500−1.312−0.0110.1713.606 × 10−51.953 × 10−8−2.255 × 10−12
500600−1.383−0.1250.1533.328 × 10−59.254 × 10−8−1.177 × 10−12
500700−1.735−0.5170.1562.393 × 10−52.309 × 10−8−8.075 × 10−14
500900−1.395−0.0820.1016.065 × 10−5−8.031 × 10−87.877 × 10−13
400800−1.473−0.280.1831.347 × 10−53.689 × 10−91.185 × 10−13
450800−1.596−0.1230.1452.482 × 10−5−1.218 × 10−96.120 × 10−14
550800−2.034−1.3260.1061.407 × 10−4−1.066 × 10−84.541 × 10−13
600800−1.608−0.2321.2208.941 × 10−4−5.302 × 10−81.664 × 10−11

### Table 7.

Somaloy 500.

Values of scaling exponents and coefficients of (42) versus compaction pressure and hardening temperature, a selection from .

Therefore, the considered binary relation is the strong inequality and corresponds to natural order presented in Figures 15 and 16. The most important question of this research is whether (45) is invariant with respect to scaling:

Ptot1'Bm1'β1>Ptot2'Bm2'β2.E46

Let λ > 0 be an arbitrary positive real number. Then, the scaling of (46) goes according to the following algorithm:

• Let us perform the scaling with respect to λ of all independent magnitudes and the dependent one:

fi=λaifi;Bmi=λbiBmi;Ptot=λciPtot,E47

where i = 1, 2 …4 labels the considered characteristics.

• Substituting appropriate relations of (47) to (48), we derive:

Ptot1Bm1β1λc1b1β1>Ptot2Bm2β2λc2b2β2.E48

• Collecting all powers of λ on the left-hand side of (48) and taking into account (43) we derive that the resulting power has to be equal zero:

λc1b1β1c2+b2β2=1.E49

Therefore, (45) is invariant with respect to scaling. This binary relation has mathematical meaning and constitutes the total order in the set of characteristics.

Binary equivalence relations. The result derived in subsection Scaling of binary relations can be supplemented with the following binary equivalence relation. Let

Xi,j=(fi,jBmi,jαi,Ptoti,jBmi,jβi)E50

be the jth point of the ith characteristic. Two points, j and k, are related if they belong to the same ith characteristic:

Xi,jXi,k.E51

Theorem: R is equivalence relation. (The proof is trivial and can be done by checking out that the considered relation is reflexive, symmetric and transitive.) Therefore, R constitutes division of the positive-positive quarter of plane spanned by (50). The characteristics do not intersect each other except in the origin point which is excluded from the space. The result of this section implies that the power losses characteristics (27) and (42) are invariant with respect to scaling. Structure of derived here the set of all characteristics of which some examples are presented in Figures 15 and 16 enable us to derive a formal pseudo-state equation of SMC. This equation constitutes a relation of the hardening temperature, the compaction pressure and a parameter characterizing the power losses characteristics corresponding to the values of these technological parameters. Finally, the pseudo-state equation will improve the algorithm for designing the best values of technological parameters.

Pseudo-equation of state for SMC. Let Cis set of all possible power losses characteristics in considered SMC. Each characteristic is smooth curve in [f/(Bm)α, Ptot/(Bm)β] plane which corresponds to a point in [T, p] plane. In order to derive the pseudo-state equation, we transform each power losses characteristic into a number V corresponding to (T, p) point. By this way, we obtain a function of two variables:

(T,p)V.E52

This function must satisfy the following condition. Let us concentrate our attention at the two following points:

f1Bm1α1=fBmα;f2Bm2α2=fBmα.E53

Let us consider the two characteristics Ptot1/(Bm1)β1and Ptot2/(Bm2)β2of the two samples composed in T1, p1 and T2, p2 temperatures and pressures, respectively, while the other technological parameters such as powder compositions and volume fraction are constant. Let us assume that for (53), the following relation holds:

Ptot1Bm1β1>Ptot2Bm2β2E54

It results from the derived structure of that (54) holds for each value of (53).Therefore, we have to assume the following condition of sought V(T, p). If the relation (54) holds for given values of temperature and pressure T1, p1, T2, p2, then the following relation for V(T, p) has to be satisfied:

V(T1,p1)>V(T2,p2).E55

Moreover, V (T, p) has to indicate place of corresponding characteristic in the ordered set. The simplest choice satisfying these requirements is the following average:

V(T,p)=1φmaxφminφminφmaxPtot(fBmα)Bmβd(fBmα),E56

The integration domain is common for all characteristics. We have selected the following common domain for the data presented in Figures 15 and 16 φmin = 0, φmax = 4000 (s−1Tα).

Using (42), we transform (56) to the working formula for the V we measure:

V(T,p)=1𝜑max𝜑min𝜑min𝜑maxx(Γ1+x(Γ2+x(Γ3+xΓ4)))dx.E57

TpV
[K][MPa][W kg−1T−β]
723.1580040.60
773.1590043.75
773.1570047.25
673.1580050.30
773.1560057.12
823.1580081.50
773.1550089.28
742.15764492.3
753.15780509.2
804.15764528.5
711.15764547.0
873.15800720.0

### Table 8.

V measure versus hardening temperature and compaction pressure.

where x=fBmαand Γi are coefficients dependent on T and p (see Table 7). The values of V (T, p) are tabulated in Table 8. Table 8 enables us to draw pseudo-isotherm. It is presented in Figure 17. However, in order to derive the complete pseudo-state equation, we must create a mathematical model. On the basis of Figure 17, we start from the classical gas state equation as an initial approximation:

pVkBT=1.E58 Figure 17.Pseudo-isotherm T = 500°C of the low-losses phase, according to data of Table 8. for Somaloy 500 .

where kB is the pseudo-Boltzmann constant.

In order to extend (58) to a realistic equation, we apply again the scaling hypothesis (27):

V(TTc,ppc)=(ppc)γΦ(TTc(ppc)δ).E59

where Φ() is an arbitrary function to be determined. Parameters γ, δ and Tc, pc are scaling exponents and scaling parameters, respectively, to be determined. For our conveniences, we introduce the following variables:

τ=(TTc);π=ppc;X=TTc(ppc)δ=τπδ.E60

In order to extend (58) to a full-state equation, we apply the Padé approximant by analogy to virial expansion derived by :

V(τ,π)=πγG0+X(G1+X(G2+X(G3+XG4)))1+X(D1+X(D2+X(D3+XD4))),E61

where G0,…, G4, D1,… D4 are coefficients of the Padé approximant. All parameters have to be determined from the data presented in Table 8.

Estimation of parameters for pseudo-equation of state. At the beginning, we have to notice that the data collected in Table 8 reveal sudden change of V between two points: [773, 15; 500, 0] and [742, 15; 764, 0]. This suggests existence of a crossover between two phases: low-losses phase and high-losses phase. We take this effect into account and we divide the data of Table 8 into two subsets corresponding to these two phases, respectively. Since the crossover consists in changing of characteristic exponents for the given universality class, it is necessary to perform estimations of the model parameters for each phase separately. Minimizations of χ2 for both phases have been performed by using MICROSOFT EXCEL 2010, where

χ2=i=1N(V(τi,πi)πiγG0+Xi(G1+Xi(G2+Xi(G3+XiG4)))1+Xi(D1+Xi(D2+Xi(D3+XiD4))))2.E62

γδTcpcG0G1G2
1.28120.171521.62237.729370315315−477522511734952
G3G4D1D2D3D4
−1.3764−678.26170.806243.8386.96−28.699

### Table 9.

Somaloy 500, low-losses phase.

Values of pseudo-state equation’s parameters and the Padé approximant’s coefficients of (61)

γδTcpcG0G1G2
1.55500.181022.94930.197365210688−477142071762773
G3G4D1D2D3D4
−1.3763−683.38170.775739.9387.81−22.514

### Table 10.

Somaloy 500, high-losses phase.

Values of pseudo-state equation’s parameters and the Padé approximant’s coefficients of (61)

where N = 7 and N = 5 for the low-losses and high-losses phases, respectively. Tables 9 and 10 present estimated values of the model parameters for the low-losses and high-losses phases, respectively.

Optimization of technological parameters. Function V (T, p) serves a power loss measure versus the hardening temperature and compaction pressure. In order to explain how to optimize the technological parameters with the pseudo-state Eq. (61), we plot the phase diagram of considered SMC Figure 17. Note that all losses’ characteristics collapsed to a one curve for the each phase. Taking into account the low-losses phase, we determine the lowest losses at τπδ = 19, 75 (see Figure 18). This gives the following continuous subspace of the optimal points:

TTc(ppc)δ=19,75.E63

Formula (63) represents the minimal iso-power loss curve. All points satisfying (63) are solutions of the optimization problem for technical parameters of SMC. By introducing the binary relations, we have revealed twofold. The power losses characteristics do not cross each other which makes the topology’s set of these curves very useful and effectively that we can perform all calculations in the one-dimensional space spanned by the scaled frequency or here in the case of pseudo-state equation in the scaled temperature. For general knowledge concerning such a topology, we refer to the paper . The obtained result is the continuous set of points satisfying (63). All solutions of these equations are equivalent for the optimization of the power losses. Therefore, the remaining degree of freedom can be used for optimizing the magnetic properties of the considered SMC.

## 6. Scaling conception of losses separation

In this section, we show how to expand losses into polynomial series. The distinction between different eddy current scales, that is a macroscale, covering the whole bulk material and a microscale covering the area of moving domain walls, introduced by Bertotti’s theory, has led to the following relationship of the three terms:

Ptot=c1fBmβ+c2σf2Bm2+8(σGSV0)f1.5Bm1.5,E64

where σ is conductivity, G is the constant equal to 0.1356; S is sample cross section, whereas V0 is a parameter dependent on flux density. In general case, (64) is not homogenous expression; therefore, this can describe the self-similarity property only for β = 1. However, the Bertotti interpretation of each term is correct

Ptot=Phys+Pclas+Pexc.E65

where the presented in (65) components are hysteresis, classical and excess losses, respectively.

In this chapter, we have shown how the two-component formula for losses (28) can be transformed to dimensionless expression (30) and (31). This expression helps us to consider the data collapse. However, in the case of expansion of (27) over the square term, (31) does not apply.

Then, one can consider partial data collapses in the expansions up to necessary degree. Let us consider, for example, (42):

PtotBmβ=(Γ1·(f/Bmα+Γ2·(f/Bmα)2+Γ3·(f/Bmα)3+Γ4·(f/Bmα)4),

Formula (42) is the fourth-degree polynomial of the (f/Bmα)scaled frequency. Let us span all possible binomial subspaces:

={S12,S13,S14,S23,S24,S34}

where Sij={(f/(Bmα))i,(f/(Bmα))j}.To consider partial data collapse in S12, we perform the following transformations:

Ptot1,2=Γ2PtotΓ12Bmβ,f1,2=Γ2fΓ1BmαE66

Substituting (66) to (42), we get

Ptot1,2(f1,2)=f1,2(1+f1,2)+f1,23Γ1Γ22(Γ3+f1,2Γ1Γ4Γ2).E67

Note that (67) is dimensionless full formula for the scaled loss. Moreover, expression f12(1 + f12) is sample independent. The linear and square terms describe the hysteresis and the classical losses, respectively. The cubic and the fourth-order terms correspond to the excess losses. Moreover, the square and linear terms describe the partial data collapse in S12 . Using (67), one can compare losses data of different measurements projected on S12 subspace. The analogical equations for the S34 subspace read:

Ptot3,4=Γ43PtotΓ34Bmβ,f3,4=Γ4fΓ3BmαE68
Ptot3,4(f3,4)=f3,43(1+f3,4)+f3,4Γ42Γ33Γ1+f3,4Γ2Γ3Γ4).E69

SampleαβΓ1Γ2Γ3Γ4
P1−2.347−1.4072.25E-037.96E-06−5.19E-091.76E-12
P2−1.519−0.3752.53E-036.79E-06−6.48E-092.78E-12
P4−2.372−1.2951.80E-022.04E-057.68E-09−1.37E-12
P7−2.437−1.4012.28E-031.05E-053.08E-07−8.38E-10

### Table 11.

Scaling exponents and expansion coefficients.

Applying (68) and (69), one can complete the data comparison by considering partial data collapse using f3,43(1+f3,4)polynomial which is also sample independent. In the case of expansion (42), the comparisons performed in S12, S34 spaces are completed. To test the presented comparison formalism, we present the following measurement data: P1—amorphous alloy Fe78Si13B9, P2—amorphous alloy Co71.5Fe2.5Mn2Mo1Si9B14, P4—crystalline material-oriented electrotechnical steel shits 3% Si-Fe and P7—iron-nickel-alloy 79%Ni-Fe. Processed measurement data in the form of scaling exponents and expansion coefficients are presented in Table 11:

Figures 19 and 20 present the completed partial collapses for the considered problem:

In order to make a numerical comparison of the measurement qualities taken from different samples, one can introduce analogically to (32) the measures of uncertainty for the both spaces S12and S34. The comparisons must be done and interpreted independently for S12and S34. Qualitative analysis on the basis of Figures 19 and 20 shows that the uncertainty measure of S34for the sample P4 is significantly high.

## 7. Summary

We have presented many examples of the measurements of power losses in soft magnetic materials, including composites. Moreover, working conditions were determined by multidimensional parameter space: frequency, pick of induction, DC bias and temperature. On the basis of obtained results of experimental and theoretical considerations, we confirm that the total power loss in soft magnetic materials is self-similar. This is very important for practices, since the fundamental parameter used by technologists in the processes aimed at tailoring properties of magnetic materials as well as in design and work analysis of magnetic circuits is loss density. However, there is one important detail which has to be discussed at the end. In order to determine F(⋅) in (27), the Maclaurin expansion has been applied up to the second-order term. Note that each two-term formula can be reduced to dimensionless form (28). Therefore, one could conclude that the data collapse is trivial. However, this is not so because relevance of the data collapse depends on measurement data. If data transformed by (30) get place on (31), then these data satisfy the axioms of homogeneity, they are invariant with respect to scaling as well as they are self-similar. What to do if the two-term expansion (28) is not sufficient? Then, one should extend (28) up to sufficient polynomial order. For an example, see (42). In general case, reduction of losses characteristic to dimensionless form is not possible. However, for comparison of different measurement data, it is possible always to perform transformation of data to dimensionless magnitudes partially in the two-dimensional subspaces (67), (69) and obtain full comparison by collecting the all independent comparisons in Sij subspaces.

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Krzysztof Z. Sokalski, Barbara Ślusarek and Jan Szczygłowski (August 24th 2016). Scaling in Magnetic Materials, Magnetic Materials, Khan Maaz, IntechOpen, DOI: 10.5772/63285. Available from:

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#### Synthesis of Silver Nanoparticles

By Remziye Güzel and Gülbahar Erdal

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